3-phenyl-4-[1,2,4]triazol-1-yl-butyraldehyde

Base Information

Chemical Name:3-phenyl-4-[1,2,4]triazol-1-yl-butyraldehyde
CAS No.:413603-72-2
Molecular Formula:C₁₂H₁₃N₃O
Molecular Weight:215.255
Hs Code.:

Synonyms:

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Chemical Property of 3-phenyl-4-[1,2,4]triazol-1-yl-butyraldehyde

Chemical Property:

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Technology Process of 3-phenyl-4-[1,2,4]triazol-1-yl-butyraldehyde

There total 4 articles about 3-phenyl-4-[1,2,4]triazol-1-yl-butyraldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79109-00-5
1-(2-phenyl-pent-4-enyl)-1H-[1,2,4]triazole

: 413603-72-2
3-phenyl-4-[1,2,4]triazol-1-yl-butyraldehyde

Guidance literature:: 1-(2-phenyl-pent-4-enyl)-1H-[1,2,4]triazole; With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In acetone; tert-butyl alcohol;

With sodium periodate; In tetrahydrofuran;
DOI:10.1016/S0960-894X(01)00655-2

Reference yield:

: 103-82-2
phenylacetic acid

: 413603-72-2
3-phenyl-4-[1,2,4]triazol-1-yl-butyraldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: LiHMDS / tetrahydrofuran / -78 °C

1.2: tetrahydrofuran / -78 - 20 °C

2.1: LAH / tetrahydrofuran

3.1: (CF₃SO₂)O; 2,6-lutidine / CH₂Cl₂

4.1: aq. OsO₄; 4-methylmorpholine N-oxide / 2-methyl-propan-2-ol; acetone

4.2: NaIO₄ / tetrahydrofuran

With 2,6-dimethylpyridine; osmium(VIII) oxide; lithium aluminium tetrahydride; trifluoromethylsulfonic anhydride; 4-methylmorpholine N-oxide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; acetone; tert-butyl alcohol;
DOI:10.1016/S0960-894X(01)00655-2

Reference yield:

: 1575-70-8
2-phenyl-pent-4-enoic acid

: 413603-72-2
3-phenyl-4-[1,2,4]triazol-1-yl-butyraldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: LAH / tetrahydrofuran

2.1: (CF₃SO₂)O; 2,6-lutidine / CH₂Cl₂

3.1: aq. OsO₄; 4-methylmorpholine N-oxide / 2-methyl-propan-2-ol; acetone

3.2: NaIO₄ / tetrahydrofuran

With 2,6-dimethylpyridine; osmium(VIII) oxide; lithium aluminium tetrahydride; trifluoromethylsulfonic anhydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; acetone; tert-butyl alcohol;
DOI:10.1016/S0960-894X(01)00655-2