Pd((C₆H₅)2PC₅H₄)2FeC₄H₃ON(C₆H₄CH₃)2

Base Information

• Chemical Name: Pd((C₆H₅)2PC₅H₄)2FeC₄H₃ON(C₆H₄CH₃)2
• CAS No.: 600174-33-2
• Molecular Formula: C₅₂H₄₅FeNOP₂Pd
• Molecular Weight: 924.15

Synonyms:

Chemical Property of Pd((C₆H₅)2PC₅H₄)2FeC₄H₃ON(C₆H₄CH₃)2

Chemical Property:

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Technology Process of Pd((C₆H₅)2PC₅H₄)2FeC₄H₃ON(C₆H₄CH₃)2

There total 1 articles about Pd((C₆H₅)2PC₅H₄)2FeC₄H₃ON(C₆H₄CH₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

potassium di(p-tolyl)amide + Pd((C6H5)2PC5H4)2FeBrC4H3O (600174-27-4) → Pd((C6H5)2PC5H4)2FeC4H3ON(C6H4CH3)2 (600174-33-2)

Guidance literature:

In toluene; (inert atm.); addn. of toluene to a mixt. of palladium complex and ligand, stirring; filtration through Celite, concn., layering with pentane, keeping at -40°C for 24 h, removal of supernatant, washing ppt. with pentane, drying in vac.; elem. anal.;

DOI:10.1021/om030257g

Reference yield:

Pd((C6H5)2PC5H4)2FeC4H3ON(C6H4CH3)2 (600174-33-2) + triphenylphosphine (603-35-0) → bis[1,2-bis(diphenylphosphino)ferrocene]-palladium(0) + Pd(PPh3)n

Guidance literature:

In benzene-d6; byproducts: furan, C4H3ONCH3C6H5, C6H5NCHNCH3C6H5; (inert atm.); heating palladium complex in C6D6 in the presence of phosphine at 100°C;

DOI:10.1021/om030257g

upstream raw materials:

Pd((C₆H₅)2PC₅H₄)2FeBrC₄H₃O

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