C₃₀H₄₂N₂O₄

Base Information

Chemical Name:C₃₀H₄₂N₂O₄
CAS No.:1404377-87-2
Molecular Formula:C₃₀H₄₂N₂O₄
Molecular Weight:494.674
Hs Code.:

C<sub>30</sub>H<sub>42</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₃₀H₄₂N₂O₄

Chemical Property:

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Technology Process of C₃₀H₄₂N₂O₄

There total 30 articles about C₃₀H₄₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 646-07-1
4-Methylpentanoic acid

: 1404377-87-2
C₃₀H₄₂N₂O₄

Guidance literature:: Multi-step reaction with 19 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

2.1: 1,1,3,3-Tetramethyldisiloxane / (Ph₃P)2IrCl(CO) / toluene / 2 h / 20 °C

3.1: hydroquinone / acetonitrile / 95 °C

4.1: methyl p-toluene sulfonate / water / 2 h / 110 °C

4.2: 4 h / 95 °C

5.1: hydrogen / rhodium contaminated with carbon / tetrahydrofuran / 7 h / 20 °C / 760.05 Torr

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

7.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

7.2: Cooling with ice

8.1: triphenylphosphine / dichloromethane / 0.33 h / Cooling with ice

8.2: 0.33 h / Cooling with ice

9.1: n-butyllithium / tetrahydrofuran

10.1: 1H-imidazole / N,N-dimethyl-formamide

11.1: pyridine / methanol

12.1: Iodine monochloride / dichloromethane

13.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water

14.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran

15.1: sodium hydrogencarbonate; Dess-Martin periodane / chloroform

16.1: toluene; methanol

17.1: trifluoroacetic acid / chloroform

18.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

19.1: hydrogen bromide; acetic acid / water

With pyridine; 1H-imidazole; potassium phosphate; n-butyllithium; 1,1,3,3-Tetramethyldisiloxane; tetrabutyl ammonium fluoride; hydrogen bromide; hydrogen; Iodine monochloride; diisobutylaluminium hydride; sodium hydrogencarbonate; benzotriazol-1-ol; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinone; methyl p-toluene sulfonate; triphenylphosphine; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; rhodium contaminated with carbon; (Ph₃P)2IrCl(CO); In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 96556-40-0
methyl-3-(benzyloxy)-2.2-dimethylpropionate

: 1404377-87-2
C₃₀H₄₂N₂O₄

Guidance literature:: Multi-step reaction with 20 steps

1: lithium borohydride / tetrahydrofuran

2: triethylamine; pyridine-SO₃ complex / dichloromethane; dimethyl sulfoxide

3: toluene

4: sodium tetrahydroborate; methanol / cobalt(II) chloride hexahydrate / N,N-dimethyl-formamide

5: sodium hydroxide / ethanol

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / chloroform

7: tetrahydrofuran

8: palladium on activated charcoal / tetrahydrofuran

9: potassium tert-butylate / toluene

10: n-butyllithium / tetrahydrofuran

11: 1H-imidazole / N,N-dimethyl-formamide

12: pyridine / methanol

13: Iodine monochloride / dichloromethane

14: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water

15: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran

16: sodium hydrogencarbonate; Dess-Martin periodane / chloroform

17: toluene; methanol

18: trifluoroacetic acid / chloroform

19: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

20: hydrogen bromide; acetic acid / water

With pyridine; 1H-imidazole; methanol; dmap; sodium tetrahydroborate; potassium phosphate; lithium borohydride; n-butyllithium; pyridine-SO₃ complex; tetrabutyl ammonium fluoride; hydrogen bromide; Iodine monochloride; sodium hydrogencarbonate; benzotriazol-1-ol; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; cobalt(II) chloride hexahydrate; palladium on activated charcoal; potassium tert-butylate; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 14002-80-3
Methyl 2,2-dimethyl-3-hydroxypropionate

: 1404377-87-2
C₃₀H₄₂N₂O₄

Guidance literature:: Multi-step reaction with 21 steps

1: diethyl ether

2: lithium borohydride / tetrahydrofuran

3: triethylamine; pyridine-SO₃ complex / dichloromethane; dimethyl sulfoxide

4: toluene

5: sodium tetrahydroborate; methanol / cobalt(II) chloride hexahydrate / N,N-dimethyl-formamide

6: sodium hydroxide / ethanol

7: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / chloroform

8: tetrahydrofuran

9: palladium on activated charcoal / tetrahydrofuran

10: potassium tert-butylate / toluene

11: n-butyllithium / tetrahydrofuran

12: 1H-imidazole / N,N-dimethyl-formamide

13: pyridine / methanol

14: Iodine monochloride / dichloromethane

15: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water

16: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran

17: sodium hydrogencarbonate; Dess-Martin periodane / chloroform

18: toluene; methanol

19: trifluoroacetic acid / chloroform

20: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

21: hydrogen bromide; acetic acid / water

With pyridine; 1H-imidazole; methanol; dmap; sodium tetrahydroborate; potassium phosphate; lithium borohydride; n-butyllithium; pyridine-SO₃ complex; tetrabutyl ammonium fluoride; hydrogen bromide; Iodine monochloride; sodium hydrogencarbonate; benzotriazol-1-ol; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; cobalt(II) chloride hexahydrate; palladium on activated charcoal; potassium tert-butylate; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;