Technology Process of acetyl 2-O-acetyl-4,6-O-benzylidene-3-O-methyl-α-D-mannopyranoside
There total 5 articles about acetyl 2-O-acetyl-4,6-O-benzylidene-3-O-methyl-α-D-mannopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium tert-butylate / N,N-dimethyl-formamide / 2.5 h / 95 °C
1.2: 20 °C
2.1: pyridine / 20 °C
With
pyridine; potassium tert-butylate;
In
N,N-dimethyl-formamide;
DOI:10.1021/ja3001584
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.67 h / 20 °C
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C
2.2: 3.5 h / 20 °C
3.1: potassium tert-butylate / N,N-dimethyl-formamide / 2.5 h / 95 °C
3.2: 20 °C
4.1: pyridine / 20 °C
With
pyridine; potassium tert-butylate; tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja3001584
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C
1.2: 3.5 h / 20 °C
2.1: potassium tert-butylate / N,N-dimethyl-formamide / 2.5 h / 95 °C
2.2: 20 °C
3.1: pyridine / 20 °C
With
pyridine; potassium tert-butylate; sodium hydride;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja3001584
