GaI₂(2,6-bis[1-[(2,5-di(isopropyl)phenyl)imino]benzyl]pyridine)

Base Information

• Chemical Name: GaI₂(2,6-bis[1-[(2,5-di(isopropyl)phenyl)imino]benzyl]pyridine)
• CAS No.: 1218775-91-7
• Molecular Formula: C₄₃H₄₇GaI₂N₃
• Molecular Weight: 929.398
• Mol file: 1218775-91-7.mol

Synonyms:

Chemical Property of GaI₂(2,6-bis[1-[(2,5-di(isopropyl)phenyl)imino]benzyl]pyridine)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of GaI₂(2,6-bis[1-[(2,5-di(isopropyl)phenyl)imino]benzyl]pyridine)

There total 1 articles about GaI₂(2,6-bis[1-[(2,5-di(isopropyl)phenyl)imino]benzyl]pyridine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

gallium(I) iodide + 2,6-bis[1-[(2,6-di(iso-propyl)phenyl)imino]-benzyl]pyridine (301658-93-5) → GaI2(2,6-bis[1-[(2,5-di(isopropyl)phenyl)imino]benzyl]pyridine) (1218775-91-7) + [GaI2(2,6-bis[1-[(2,5-di(isopropyl)phenyl)imino]benzyl]pyridine)GaI4] (1218775-90-6)

Guidance literature:

In toluene; (under N2); GaI added to soln. of ligand in toluene, sealed, stirred for6 h at room temp., cooled to -20°C overnight; filtered, washed with hexane, dried under vac.; elem. anal.;

DOI:10.1039/b920047a

upstream raw materials:

2,6-bis[1-[(2,6-di(iso-propyl)phenyl)imino]-benzyl]pyridine