tert-butyl 5-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-6-deoxy-2,3-O-isopropylidene-6-(4-octylphenylureido)-1-(uracil-1-yl)-β-D-glycero-L-talo-heptofuranuronate

Base Information

• Chemical Name: tert-butyl 5-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-6-deoxy-2,3-O-isopropylidene-6-(4-octylphenylureido)-1-(uracil-1-yl)-β-D-glycero-L-talo-heptofuranuronate
• CAS No.: 1223563-65-2
• Molecular Formula: C₄₈H₇₃N₅O₁₄
• Molecular Weight: 944.133

Synonyms:

Chemical Property of tert-butyl 5-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-6-deoxy-2,3-O-isopropylidene-6-(4-octylphenylureido)-1-(uracil-1-yl)-β-D-glycero-L-talo-heptofuranuronate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tert-butyl 5-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-6-deoxy-2,3-O-isopropylidene-6-(4-octylphenylureido)-1-(uracil-1-yl)-β-D-glycero-L-talo-heptofuranuronate

There total 1 articles about tert-butyl 5-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-6-deoxy-2,3-O-isopropylidene-6-(4-octylphenylureido)-1-(uracil-1-yl)-β-D-glycero-L-talo-heptofuranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-3-[6-(tert-butoxycarbonylamino-methyl)-2,2-diethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yloxy]-3-[6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl]-propionic acid tert-butyl ester (935560-23-9) + 1-isocyanato-4-octylbenzene → tert-butyl 5-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-6-deoxy-2,3-O-isopropylidene-6-(4-octylphenylureido)-1-(uracil-1-yl)-β-D-glycero-L-talo-heptofuranuronate (1223563-65-2)

Guidance literature:

In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/jm100243n

Reference yield: 93.0%

tert-butyl 5-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-6-deoxy-2,3-O-isopropylidene-6-(4-octylphenylureido)-1-(uracil-1-yl)-β-D-glycero-L-talo-heptofuranuronate (1223563-65-2) + trifluoroacetic acid (76-05-1) → 5-O-(5-amino-5-deoxy-β-D-ribofuranosyl)-6-deoxy-6-(4-octylphenylureido)-1-(uracil-1-yl)-β-D-glycero-L-talo-heptofuranuronic acid trifluoroacetate salt (1223563-51-6)

Guidance literature:

In water; at 20 ℃; for 6h;

DOI:10.1021/jm100243n

upstream raw materials:

2-amino-3-[6-(tert-butoxycarbonylamino-methyl)-2,2-diethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yloxy]-3-[6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl]-propionic acid tert-butyl ester

Downstream raw materials:

5-O-(5-amino-5-deoxy-β-D-ribofuranosyl)-6-deoxy-6-(4-octylphenylureido)-1-(uracil-1-yl)-β-D-glycero-L-talo-heptofuranuronic acid trifluoroacetate salt

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