Co(CNC₆H₅)3(P(C₆H₁₃)3)2⁽¹⁺⁾*ClO₄^(1-) = Co(CNC₆H₅)3(P(C₆H₁₃)3)2(ClO₄)

Base Information

• Chemical Name: Co(CNC₆H₅)3(P(C₆H₁₃)3)2⁽¹⁺⁾*ClO₄^(1-) = Co(CNC₆H₅)3(P(C₆H₁₃)3)2(ClO₄)
• CAS No.: 94698-32-5
• Molecular Formula: C₅₇H₉₃CoN₃P₂*ClO₄
• Molecular Weight: 1040.78
• Mol file: 94698-32-5.mol

Synonyms:

Chemical Property of Co(CNC₆H₅)3(P(C₆H₁₃)3)2⁽¹⁺⁾*ClO₄^(1-) = Co(CNC₆H₅)3(P(C₆H₁₃)3)2(ClO₄)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Co(CNC₆H₅)3(P(C₆H₁₃)3)2⁽¹⁺⁾*ClO₄^(1-) = Co(CNC₆H₅)3(P(C₆H₁₃)3)2(ClO₄)

There total 1 articles about Co(CNC₆H₅)3(P(C₆H₁₃)3)2⁽¹⁺⁾*ClO₄^(1-) = Co(CNC₆H₅)3(P(C₆H₁₃)3)2(ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

pentakis(phenylisocyanide)cobalt(I)(1+) perchlorate * chloroform (53495-85-5,50308-13-9) + trihexylphosphine (4168-73-4) → Co(CNC6H5)3(P(C6H13)3)2(1+)*ClO4(1-) = Co(CNC6H5)3(P(C6H13)3)2(ClO4) (94698-32-5)

Guidance literature:

In dichloromethane; Cold phopshine (5:1 molar ratio) was added dropwise to a soln. of complex cooled in ice, 60 min;; Treated with ether, chilled in ice 90 min, left overnight in a cold room at 7°C, recrystd. from CH2Cl2-Et2O; elem. anal.;

DOI:10.1016/S0020-1693(00)82440-8

upstream raw materials:

pentakis(phenylisocyanide)cobalt(I)⁽¹⁺⁾ perchlorate * chloroform

trihexylphosphine