[Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]BPh₄

Base Information

Chemical Name:[Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]BPh₄
CAS No.:691879-56-8
Molecular Formula:C₂₄H₂₀B*C₄₃H₇₅N₂OP₂Ru
Molecular Weight:1118.33
Hs Code.:

[Ru(CH=CH<sub>2</sub>)(CO)(NCCH<sub>3</sub>)2(P(Cy)3)2]BPh<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]BPh₄

Chemical Property:

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Technology Process of [Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]BPh₄

There total 1 articles about [Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]BPh₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 691879-50-2
[Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]PF₆

: 143-66-8
sodium tetraphenyl borate

: 691879-56-8
[Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]BPh₄

Guidance literature:: In methanol; under Ar; a suspn. of Ru-contg. compd. (0.12 mmol) in methanol was treated with NaBPh4 (0.73 mmol) and stirred for 1 h at room temp.; the solvent was evapd. in vac. and the residue was washed twice with methanol and then dissolved in CH2Cl2; the soln. was filtered and the filtrate was brought to dryness in vac.; the solid was washed twice with pentane and dried; elem. anal.;
DOI:10.1039/b314425a

Reference yield: 90.0%

: tetrafluoroboric acid

: 691879-56-8
[Ru(CH=CH₂)(CO)(NCCH₃)2(P(Cy)3)2]BPh₄

: [(Cy)3PCH=CH₂]BF₄

Guidance literature:: In diethyl ether; dichloromethane; under Ar; a soln. of Ru-contg. compd. (0.04 mmol) in CH2Cl2 was treated with a soln. of HBF4 in diethyl ether (0.16 mmol) at room temp.; stirring for 5 min; the solvent was evaps. in vac.; the residue was washed twice with pentane and dried; some by-products were formed; detd. by by (1)H and (31)P NMR studies;
DOI:10.1039/b314425a