C₁₃H₁₉NO₃

Base Information

Chemical Name:C₁₃H₁₉NO₃
CAS No.:1280563-48-5
Molecular Formula:C₁₃H₁₉NO₃
Molecular Weight:237.299
Hs Code.:

C<sub>13</sub>H<sub>19</sub>NO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₉NO₃

Chemical Property:

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Technology Process of C₁₃H₁₉NO₃

There total 4 articles about C₁₃H₁₉NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₁₇NO₃

: 1280563-48-5
C₁₃H₁₉NO₃

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In acetonitrile; at 0 ℃; for 1h; stereoselective reaction;
DOI:10.5012/bkcs.2010.31.12.3794

Reference yield:

: C₂₅H₄₅NO₃Si₂

: 1280563-48-5
C₁₃H₁₉NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

2: sodium tris(acetoxy)borohydride; acetic acid / acetonitrile / 1 h / 0 °C

With tetrabutyl ammonium fluoride; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.5012/bkcs.2010.31.12.3794

Reference yield:

: 1280563-30-5
N-methyl-2-iodo-5-methylphenylamine

: 1280563-48-5
C₁₃H₁₉NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: tributyl-amine; triphenyl-arsane; palladium diacetate / N,N-dimethyl-formamide / 24 h / 70 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

3: sodium tris(acetoxy)borohydride; acetic acid / acetonitrile / 1 h / 0 °C

With tributyl-amine; triphenyl-arsane; tetrabutyl ammonium fluoride; palladium diacetate; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile; 1: Heck-type coupling reaction;
DOI:10.5012/bkcs.2010.31.12.3794