tert-butyl N-(1S,2R)-3-[[(3-aminophenyl)sulfonyl] (cyclopentyl oxy)amino]-1-benzyl-2-hydroxypropylcarbamate

Base Information

Chemical Name:tert-butyl N-(1S,2R)-3-[[(3-aminophenyl)sulfonyl] (cyclopentyl oxy)amino]-1-benzyl-2-hydroxypropylcarbamate
CAS No.:252870-86-3
Molecular Formula:C₂₆H₃₇N₃O₆S
Molecular Weight:519.662
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl N-(1S,2R)-3-[[(3-aminophenyl)sulfonyl] (cyclopentyl oxy)amino]-1-benzyl-2-hydroxypropylcarbamate

Chemical Property:

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Technology Process of tert-butyl N-(1S,2R)-3-[[(3-aminophenyl)sulfonyl] (cyclopentyl oxy)amino]-1-benzyl-2-hydroxypropylcarbamate

There total 2 articles about tert-butyl N-(1S,2R)-3-[[(3-aminophenyl)sulfonyl] (cyclopentyl oxy)amino]-1-benzyl-2-hydroxypropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 252870-86-3
tert-butyl N-(1S,2R)-3-[[(3-aminophenyl)sulfonyl] (cyclopentyl oxy)amino]-1-benzyl-2-hydroxypropylcarbamate

Guidance literature:

Reference yield:

: 252872-71-2
3-amino-N₁-(cyclopentyloxy)-1-benzenesulfonamide

: 98760-08-8,98818-34-9,98818-35-0,103127-56-6,98737-29-2
(1-oxiranyl-2-phenylethyl)carbamic acid tert-butyl ester

: 252870-86-3
tert-butyl N-(1S,2R)-3-[[(3-aminophenyl)sulfonyl] (cyclopentyl oxy)amino]-1-benzyl-2-hydroxypropylcarbamate

Guidance literature:: With P₄-phosphazene; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2005.05.101

Reference yield:

: 252870-86-3
tert-butyl N-(1S,2R)-3-[[(3-aminophenyl)sulfonyl] (cyclopentyl oxy)amino]-1-benzyl-2-hydroxypropylcarbamate

: (3R,3aS,6aR)hexahydrofuro[2,3-b]furan-3-yl N-(1S,2R)-3-[[(3-aminophenyl)sulfonyl](cyclopentyloxy)amino]-1-benzyl-2-hydroxypropylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: TFA

2: DIEA / CH₂Cl₂

With N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2005.05.101