<2R^*-<2α(S^*), 3β, 11bβ>>-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2-<(2,3,4,9-tetrahydro-1H-pyrido<3,4b>indol-1-yl)methyl>-2H-benzoquinolizine

Base Information

• Chemical Name: <2R^*-<2α(S^*), 3β, 11bβ>>-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2-<(2,3,4,9-tetrahydro-1H-pyrido<3,4b>indol-1-yl)methyl>-2H-benzo
• Molecular Formula: C₃₆H₄₃N₃O₃
• Molecular Weight: 565.756

Synonyms:

Chemical Property of <2R^*-<2α(S^*), 3β, 11bβ>>-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2-<(2,3,4,9-tetrahydro-1H-pyrido<3,4b>indol-1-yl)methyl>-2H-benzo

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There total 2 articles about <2R^*-<2α(S^*), 3β, 11bβ>>-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2-<(2,3,4,9-tetrahydro-1H-pyrido<3,4b>indol-1-yl)methyl>-2H-benzoquinolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

C36H41N3O3*2BrH*H2O → <2R*-<2α(R*),3β,11bβ>>-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2-<(2,3,4,9-tetrahydro-1H-pyrido<3,4b>indol-1-yl)methyl>-2H-benzoquinolizine (65847-02-1,65878-17-3,69461-02-5,69461-03-6) + <2R*-<2α(S*), 3β, 11bβ>>-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2-<(2,3,4,9-tetrahydro-1H-pyrido<3,4b>indol-1-yl)methyl>-2H-benzoquinolizine (65847-02-1,65878-17-3,69461-02-5,69461-03-6)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 25 ℃; for 1.5h;

DOI:10.1248/cpb.33.1946

Reference yield: 18.0%

C36H41N3O3*2BrH*H2O → <2R*-<2α(R*),3β,11bβ>>-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2-<(2,3,4,9-tetrahydro-1H-pyrido<3,4b>indol-1-yl)methyl>-2H-benzoquinolizine (65847-02-1,65878-17-3,69461-02-5,69461-03-6) + <2R*-<2α(S*), 3β, 11bβ>>-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2-<(2,3,4,9-tetrahydro-1H-pyrido<3,4b>indol-1-yl)methyl>-2H-benzoquinolizine (65847-02-1,65878-17-3,69461-02-5,69461-03-6)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 25 ℃; for 1.5h;

DOI:10.1248/cpb.33.1946

Reference yield: 95.0%

<2R*-<2α(R*),3β,11bβ>>-8-benzyloxy-3-ethyl-1,3,4,6,7,11b-hexahydro-9,10-dimethoxy-2-<(2,3,4,9-tetrahydro-1H-pyrido<3,4b>indol-1-yl)methyl>-2H-benzoquinolizine (65847-02-1,65878-17-3,69461-02-5,69461-03-6) → <2R*-<2α(R*),3β,11bβ>>-3-ethyl-1,3,4,6,7,11b-hexahydro-8-hydroxy-9,10-dimethoxy-2-<(2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-2H-benzoquinolizine (13849-53-1,65847-00-9,65878-16-2,69461-04-7)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; acetic acid; at 20 ℃; for 1.5h; atmospheric pressure;

DOI:10.1248/cpb.33.1946

Downstream raw materials:

<2R^*-<2α(R^*),3β,11bβ>>-3-ethyl-1,3,4,6,7,11b-hexahydro-8-hydroxy-9,10-dimethoxy-2-<(2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-2H-benzoquinolizine

(+/-)-alangimarckine

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