4-(4'-BROMOPHENYL)PIPERIDINE HYDROCHLORIDE

Base Information

• Chemical Name: 4-(4'-BROMOPHENYL)PIPERIDINE HYDROCHLORIDE
• CAS No.: 769944-79-8
• Molecular Formula: C11H15BrClN
• Molecular Weight: 276.604
• Hs Code.: 2933399090
• Mol file: 769944-79-8.mol

Synonyms:Piperidine,4-(4-bromophenyl)-, hydrochloride (9CI);4-(4-Bromophenyl)piperidinehydrochloride;4-(4-Bromo-phenyl)piperidine HCl;4-(4-bromophenyl)piperidine hydrochloride;

Chemical Property of 4-(4'-BROMOPHENYL)PIPERIDINE HYDROCHLORIDE

Chemical Property:

• Boiling Point: 340.5 °C at 760 mmHg
• Flash Point: 159.7 °C
• PSA: 12.03000
• LogP: 4.04690
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

4-(4-Bromophenyl)piperidineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(4'-BROMOPHENYL)PIPERIDINE HYDROCHLORIDE

There total 1 articles about 4-(4'-BROMOPHENYL)PIPERIDINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

tert-butyl 4-(4-bromophenyl)piperidine-1-carboxylate (769944-78-7) → 4-(4-bromophenyl)piperidine hydrogen chloride salt (769944-79-8)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 20 ℃; for 5h;

Reference yield: 93.0%

2-chloro-3-methyl-6-(pyridin-4-yl)pyrimidin-4(3H)-one (521969-44-8) + 4-(4-bromophenyl)piperidine hydrogen chloride salt (769944-79-8) → 2-(4-(4-bromo-phenyl)-piperidin-1-yl)-3-methyl-6-pyridin-4-yl-3H-pyrimidin-4-one

Guidance literature:

With triethylamine; In tetrahydrofuran; for 3h;

Reference yield: 34.0%

4-(4-bromophenyl)piperidine hydrogen chloride salt (769944-79-8) + 6-chloro-3-methoxy-[1,2,4]triazolo[4,3-b]pyridazine → 6-(4-(4-bromophenyl)-piperidin-1-yl)-3-methoxy[1,2,4]triazolo[4,3-b]pyridazine

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 80 ℃; for 16h; Inert atmosphere;

DOI:10.1021/acs.jmedchem.6b00070

upstream raw materials:

tert-butyl 4-(4-bromophenyl)piperidine-1-carboxylate

Downstream raw materials:

tert-butyl 4-(4-bromophenyl)piperidine-1-carboxylate

4-(4-bromophenyl)-1-(2,2,2,-trifluoroethyl)piperidine

4-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1-(2,2,2-trifluoroethyl)piperidine

1-(6-(4-chloro-4'-(1-(2,2,2-trifluoroethyl)piperidin-4-yl)-[1,1'-biphenyl]-2-yl)pyridin-2-yl)-5-(trifluoromethyl)-1H-pyrazole-4-carboxylic acid

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