Technology Process of C15H19N3OS
There total 6 articles about C15H19N3OS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
methanol; acetic acid;
at 100 ℃;
for 3h;
DOI:10.1002/ejoc.201101509
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloromethane / 4.08 h / 20 °C
2: hydrogenchloride / methanol; acetic acid / 3 h / 100 °C
With
hydrogenchloride;
In
methanol; dichloromethane; acetic acid;
DOI:10.1002/ejoc.201101509
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydroxide / toluene / 4 h / 20 °C
2.1: chloroformic acid ethyl ester; triethylamine / diethyl ether / 0.17 h / -10 °C
2.2: 18 h / 0 °C
2.3: 16 h / 20 °C
3.1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 20 °C
4.1: sodium hydrogencarbonate / dichloromethane; water / 1 h / 20 °C
5.1: dichloromethane / 4.08 h / 20 °C
6.1: hydrogenchloride / methanol; acetic acid / 3 h / 100 °C
With
hydrogenchloride; palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; sodium hydroxide;
In
methanol; diethyl ether; dichloromethane; water; acetic acid; toluene;
DOI:10.1002/ejoc.201101509