(+/-)-2R^*,11bS^*-N-(2-Cyano-9,10-dimethoxy-1,3,4,6,7,11b-hexahydrobenzoquinolizin-2-yl)-N'-phenylurea

Base Information

• Chemical Name: (+/-)-2R^*,11bS^*-N-(2-Cyano-9,10-dimethoxy-1,3,4,6,7,11b-hexahydrobenzo
• Molecular Formula: C₂₃H₂₆N₄O₃
• Molecular Weight: 406.484

Synonyms:

Chemical Property of (+/-)-2R^*,11bS^*-N-(2-Cyano-9,10-dimethoxy-1,3,4,6,7,11b-hexahydrobenzo

Chemical Property:

Purity/Quality:

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Useful:

There total 1 articles about (+/-)-2R^*,11bS^*-N-(2-Cyano-9,10-dimethoxy-1,3,4,6,7,11b-hexahydrobenzoquinolizin-2-yl)-N'-phenylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

phenyl isocyanate (103-71-9) + 2-Amino-9,10-dimethoxy-1,3,4,6,7,11b-hexahydrobenzoquinolizine-2-carbonitrile (133308-74-4,136334-26-4) → (+/-)-2R*,11bS*-N-(2-Cyano-9,10-dimethoxy-1,3,4,6,7,11b-hexahydrobenzoquinolizin-2-yl)-N'-phenylurea (133308-68-6,136334-32-2)

Guidance literature:

In benzene; for 6h; Heating;

Reference yield: 60.0%

(+/-)-2R*,11bS*-N-(2-Cyano-9,10-dimethoxy-1,3,4,6,7,11b-hexahydrobenzoquinolizin-2-yl)-N'-phenylurea (133308-68-6,136334-32-2) → (+/-)-2R*,11bS*-4'-Imino-9,10-dimethoxy-3'-phenyl-1,3,4,6,7,11b-hexahydrospiroquinolizin-2,5'-imidazolidin>-2'-one (136334-38-8)

Guidance literature:

In ethanol; for 1h; Heating;

upstream raw materials:

phenyl isocyanate

2-Amino-9,10-dimethoxy-1,3,4,6,7,11b-hexahydrobenzoquinolizine-2-carbonitrile

Downstream raw materials:

(+/-)-2R^*,11bS^*-4'-Imino-9,10-dimethoxy-3'-phenyl-1,3,4,6,7,11b-hexahydrospiroquinolizin-2,5'-imidazolidin>-2'-one

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