Technology Process of (4S,6S)- and (4R,6R)-4-(3,5-dinitrobenzoyloxy)-1,7-dioxaspiro<5.5>undecan
There total 10 articles about (4S,6S)- and (4R,6R)-4-(3,5-dinitrobenzoyloxy)-1,7-dioxaspiro<5.5>undecan which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 98 percent / H2, quinoline, sodium hydrogen carbonate / Pd/BaSO4 / methanol
2: 68 percent / camphorsulphonic acid / CH2Cl2 / 0.17 h
3: 5 percent / HCl / tetrahydrofuran; H2O / 18 h
4: pyridine
With
quinoline; hydrogenchloride; camphor-10-sulfonic acid; hydrogen; sodium hydrogencarbonate;
Pd-BaSO4;
In
tetrahydrofuran; pyridine; methanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 98 percent / H2, quinoline, sodium hydrogen carbonate / Pd/BaSO4 / methanol
2: 68 percent / camphorsulphonic acid / CH2Cl2 / 0.17 h
3: 60 percent / HCl / tetrahydrofuran; H2O / 18 h
4: pyridine
With
quinoline; hydrogenchloride; camphor-10-sulfonic acid; hydrogen; sodium hydrogencarbonate;
Pd-BaSO4;
In
tetrahydrofuran; pyridine; methanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 86 percent / Amberlite resin (IR-118) / methanol / 24 h
2: 98 percent / H2, quinoline, sodium hydrogen carbonate / Pd/BaSO4 / methanol
3: 68 percent / camphorsulphonic acid / CH2Cl2 / 0.17 h
4: 5 percent / HCl / tetrahydrofuran; H2O / 18 h
5: pyridine
With
quinoline; hydrogenchloride; Amberlite resin (IR-118); camphor-10-sulfonic acid; hydrogen; sodium hydrogencarbonate;
Pd-BaSO4;
In
tetrahydrofuran; pyridine; methanol; dichloromethane; water;
