di(6-chloro-2-methylphenyl)carbazone

Base Information

• Chemical Name: di(6-chloro-2-methylphenyl)carbazone
• CAS No.: 325771-89-9
• Molecular Formula: C₁₅H₁₄Cl₂N₄O
• Molecular Weight: 337.208
• Mol file: 325771-89-9.mol

Synonyms:

Chemical Property of di(6-chloro-2-methylphenyl)carbazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of di(6-chloro-2-methylphenyl)carbazone

There total 2 articles about di(6-chloro-2-methylphenyl)carbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di(6-chloro-2-methylphenyl)carbazide → di(6-chloro-2-methylphenyl)carbazone (325771-89-9)

Guidance literature:

With dipotassium peroxodisulfate; ferric alum; sulfuric acid; In acetic acid; for 0.5h;

DOI:10.1016/S1386-1425(00)00316-4

Reference yield:

6-chloro-2-methylphenylhydrazine (89187-46-2) → di(6-chloro-2-methylphenyl)carbazone (325771-89-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 3 h / 155 - 160 °C

2: 1N H₂SO₄; 10 percent ferric alum; K₂S₂O₈ / acetic acid / 0.5 h

With dipotassium peroxodisulfate; ferric alum; sulfuric acid; In acetic acid;

DOI:10.1016/S1386-1425(00)00316-4

Reference yield:

di(6-chloro-2-methylphenyl)carbazone (325771-89-9) → bis(2-picoline)nickel(II) di(6-chloro-2-methylphenyl)carbazonate

Guidance literature:

Multi-step reaction with 2 steps

1: acetate buffer / water; ethanol

2: chloroform

With acetate buffer; In ethanol; chloroform; water;

DOI:10.1016/S1386-1425(00)00316-4

upstream raw materials:

6-chloro-2-methylphenylhydrazine