Technology Process of C58H95N17O19S
There total 21 articles about C58H95N17O19S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 81 percent / dimethylformamide / 20 h / 20 °C
2: H2 / Pd/C / methanol
3: dimethylformamide / 24 h / 20 °C
4: H2 / Pd/C / methanol
5: dimethylformamide / 15 h / 20 °C
6: CF3COOH / 1 h
7: dimethylformamide / 20 h
8: CF3COOH / 1 h
9: dimethylformamide / 15 h / 20 °C
With
hydrogen; trifluoroacetic acid;
palladium on activated charcoal;
In
methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: DCC/pentafluorophenol / dimethylformamide / 1.) -4 deg C, 1 h 2.)r.t., 5 h
2: H2 / Pd/C / dimethylformamide
3: N,N'-dicyclohexylcarbodiimide / dimethylformamide / 1.)-10 deg C, 1 h 2.)-4 deg C, 2 h 3.)20 deg C, 10 h
4: dimethylformamide / 15 h / 20 °C
With
2,3,4,5,6-pentafluorophenol; hydrogen; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: CF3COOH / 1 h
2: DCC/pentafluorophenol / dimethylformamide / 1.) -4 deg C, 1 h 2.)r.t., 5 h
3: H2 / Pd/C / dimethylformamide
4: N,N'-dicyclohexylcarbodiimide / dimethylformamide / 1.)-10 deg C, 1 h 2.)-4 deg C, 2 h 3.)20 deg C, 10 h
5: dimethylformamide / 15 h / 20 °C
With
2,3,4,5,6-pentafluorophenol; hydrogen; dicyclohexyl-carbodiimide; trifluoroacetic acid;
palladium on activated charcoal;
In
N,N-dimethyl-formamide;
