C₂₈H₂₄N₆O₇

Base Information

Chemical Name:C₂₈H₂₄N₆O₇
CAS No.:1313028-58-8
Molecular Formula:C₂₈H₂₄N₆O₇
Molecular Weight:556.535
Hs Code.:

C<sub>28</sub>H<sub>24</sub>N<sub>6</sub>O<sub>7</sub>

Synonyms:

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Chemical Property of C₂₈H₂₄N₆O₇

Chemical Property:

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Technology Process of C₂₈H₂₄N₆O₇

There total 14 articles about C₂₈H₂₄N₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₁₆N₆O₄

: 15586-16-0
4-methoxybenzyloxycarbonyl chloride

: 1313028-58-8
C₂₈H₂₄N₆O₇

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1039/c1cc11532d

Reference yield:

: 499-83-2
Pyridine-2,6-dicarboxylic acid

: 1313028-58-8
C₂₈H₂₄N₆O₇

Guidance literature:: Multi-step reaction with 9 steps

1: sulfuric acid / 48 h / Reflux

2: sodium hydroxide / water / 12 h / 20 °C

3: 4-methyl-morpholine; chloroformic acid ethyl ester / tetrahydrofuran; N,N-dimethyl-formamide / 0.25 h / -10 - -5 °C

4: sodium azide / tetrahydrofuran; water; N,N-dimethyl-formamide / 0.5 h / Cooling

5: toluene / 30 h / 120 °C

6: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 50 °C

7: triethylamine / dichloromethane / 1 h / 20 °C

8: palladium 10% on activated carbon; hydrogen / N,N-dimethyl-formamide / 20 °C

9: triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C

With 4-methyl-morpholine; sodium azide; sulfuric acid; palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c1cc11532d

Reference yield:

: 7170-36-7
6-(methoxycarbonyl)pyridine-2-carboxylic acid

: 1313028-58-8
C₂₈H₂₄N₆O₇

Guidance literature:: Multi-step reaction with 7 steps

1: 4-methyl-morpholine; chloroformic acid ethyl ester / tetrahydrofuran; N,N-dimethyl-formamide / 0.25 h / -10 - -5 °C

2: sodium azide / tetrahydrofuran; water; N,N-dimethyl-formamide / 0.5 h / Cooling

3: toluene / 30 h / 120 °C

4: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 50 °C

5: triethylamine / dichloromethane / 1 h / 20 °C

6: palladium 10% on activated carbon; hydrogen / N,N-dimethyl-formamide / 20 °C

7: triethylamine / N,N-dimethyl-formamide / 2 h / 20 °C

With 4-methyl-morpholine; sodium azide; palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c1cc11532d