Technology Process of C44H53O5PS2
There total 15 articles about C44H53O5PS2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 1.) Mg / 1.) THF, 2.) THF
2: LiAlH4
3: n-BuLi
4: H2O2
5: n-Bu4NF
6: Et3N
7: LiCl
8: K2CO3
With
lithium aluminium tetrahydride; n-butyllithium; tetrabutyl ammonium fluoride; dihydrogen peroxide; potassium carbonate; magnesium; triethylamine; lithium chloride;
- Guidance literature:
-
Multi-step reaction with 12 steps
1: H2SO4
2: LiAlH4
3: p-TsOH
4: LiAlH4
5: 1.) NaH
6: Et3N
7: n-BuLi
8: H2O2
9: n-Bu4NF
10: Et3N
11: LiCl
12: K2CO3
With
lithium aluminium tetrahydride; n-butyllithium; sulfuric acid; tetrabutyl ammonium fluoride; dihydrogen peroxide; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; triethylamine; lithium chloride;
- Guidance literature:
-
Multi-step reaction with 11 steps
1: LiAlH4
2: p-TsOH
3: LiAlH4
4: 1.) NaH
5: Et3N
6: n-BuLi
7: H2O2
8: n-Bu4NF
9: Et3N
10: LiCl
11: K2CO3
With
lithium aluminium tetrahydride; n-butyllithium; tetrabutyl ammonium fluoride; dihydrogen peroxide; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; triethylamine; lithium chloride;