(2-phenylethyl)cyclopentadienylthallium

Base Information

Chemical Name:(2-phenylethyl)cyclopentadienylthallium
CAS No.:211874-19-0
Molecular Formula:C₁₃H₁₃Tl
Molecular Weight:373.629
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-phenylethyl)cyclopentadienylthallium

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Technology Process of (2-phenylethyl)cyclopentadienylthallium

There total 1 articles about (2-phenylethyl)cyclopentadienylthallium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.5%

: (2-phenylethyl)cyclopentadiene

: 20398-06-5
thallium (I) ethoxide

: 211874-19-0
(2-phenylethyl)cyclopentadienylthallium

Guidance literature:: In diethyl ether; Ar-atmosphere; addn. of 1 equiv. of TlOEt to soln. of Cp-ligand (pptn.),addn. of Et2O, stirring for 1 h; collection (filtration), washing (pentane), drying (vac.), sublimation (90°C, 0.03 mmHg); elem. anal.;
DOI:10.1021/om980118c

Reference yield: 91.8%

: di(rhodium)tetracarbonyl dichloride

: 211874-19-0
(2-phenylethyl)cyclopentadienylthallium

: 211874-23-6
[η(5)-(2-phenylethyl)cyclopentadienyl]dicarbonylrhodium

Guidance literature:: In tetrahydrofuran; Ar-atmosphere; stirring overnight; filtration, evapn., chromy. (SiO2, hexane), evapn., distillation (110°C, 0.005 mmHg); elem. anal.;
DOI:10.1021/om980118c

Reference yield: 52.0%

: 12129-06-5
Cp*TiCl₃

: 211874-19-0
(2-phenylethyl)cyclopentadienylthallium

: 211874-25-8
[η(5)-(2-phenylethyl)cyclopentadienyl](η(5)-pentamethylcyclopentadienyl)dichlorotitanium

Guidance literature:: In benzene; Ar-atmosphere; excess of Ti-complex, stirring overnight; filtration, evapn., crystn. (MePh, hexane, -20°C); elem. anal.;
DOI:10.1021/om980118c