p-nitrophenylazo-6-methyl-4-pyrimidinylacetaldehyde oxime

Base Information

Chemical Name:p-nitrophenylazo-6-methyl-4-pyrimidinylacetaldehyde oxime
CAS No.:97189-40-7
Molecular Formula:C₁₃H₁₂N₆O₃
Molecular Weight:300.277
Hs Code.:

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Chemical Property of p-nitrophenylazo-6-methyl-4-pyrimidinylacetaldehyde oxime

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Technology Process of p-nitrophenylazo-6-methyl-4-pyrimidinylacetaldehyde oxime

There total 3 articles about p-nitrophenylazo-6-methyl-4-pyrimidinylacetaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 97189-38-3
p-nitrophenylazo-6-methyl-4-pyrimidinylacetaldehyde

: 97189-40-7
p-nitrophenylazo-6-methyl-4-pyrimidinylacetaldehyde oxime

Guidance literature:: With hydroxylamine hydrochloride;
DOI:10.1007/BF00504416

Reference yield:

: 83256-17-1
4-methyl-6-(β-dimethylaminovinyl)pyrimidine

: 97189-40-7
p-nitrophenylazo-6-methyl-4-pyrimidinylacetaldehyde oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium nitrite, conc. HCl, 2.) sodium acetate / 1.) water, 0-5 deg C, 2.) conc. HCl, pH 6.

2: 100 percent / hydroxylamine hydrochloride

With hydrogenchloride; hydroxylamine hydrochloride; sodium acetate; sodium nitrite;
DOI:10.1007/BF00504416

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 97189-40-7
p-nitrophenylazo-6-methyl-4-pyrimidinylacetaldehyde oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium nitrite, conc. HCl, 2.) sodium acetate / 1.) water, 0-5 deg C, 2.) conc. HCl, pH 6.

2: 100 percent / hydroxylamine hydrochloride

With hydrogenchloride; hydroxylamine hydrochloride; sodium acetate; sodium nitrite;
DOI:10.1007/BF00504416