{(PMe₂Ph)3Cl₂Ir(H₂O)}ClO₄

Base Information

Chemical Name:{(PMe₂Ph)3Cl₂Ir(H₂O)}ClO₄
CAS No.:106587-16-0
Molecular Formula:C₂₄H₃₅Cl₂IrOP₃*ClO₄
Molecular Weight:795.039
Hs Code.:

{(PMe<sub>2</sub>Ph)3Cl<sub>2</sub>Ir(H<sub>2</sub>O)}ClO<sub>4</sub>

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Chemical Property of {(PMe₂Ph)3Cl₂Ir(H₂O)}ClO₄

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Technology Process of {(PMe₂Ph)3Cl₂Ir(H₂O)}ClO₄

There total 1 articles about {(PMe₂Ph)3Cl₂Ir(H₂O)}ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15613-31-7,15664-86-5,21919-29-9
mer-IrCl₃(PMe₂Ph)3

: silver perchlorate

: 106587-16-0
{(PMe₂Ph)3Cl₂Ir(H₂O)}ClO₄

Guidance literature:: In acetone; byproducts: AgCl; suspn. was shaken for 40 min; AgCl is filtered off, evapd.; dissolved (CH2Cl2); pptd. (diethyl ether); elem. anal.;

Reference yield: 78.0%

: 106587-16-0
{(PMe₂Ph)3Cl₂Ir(H₂O)}ClO₄

: 149133-88-0
{IrCl₂(SH)(P(CH₃)2C₆H₅)3}

Guidance literature:: With hydrogen sulfide; In methanol; bubbling H2S gas through soln. of Ir complex in min. amt. of methanol until start of pptn.;; filtration after complete pptn.; recrystn. from CH2Cl2/diethyl ether;;
DOI:10.1039/DT9930001093

Reference yield:

: 106587-16-0
{(PMe₂Ph)3Cl₂Ir(H₂O)}ClO₄

: {IrCl₂(P(CH₃)2C₆H₅)3}⁽¹⁺⁾

Guidance literature:: In chloroform-d1; byproducts: H2O; equil. in soln. at room temp.;; not isolated; detected in soln. by (1)H and (31)P NMR spectroscopy;;
DOI:10.1039/DT9930001093