tricarbonyl[2-[tricarbonyl[η(6)-2[(phenyl-κ(2)C(1')C(2'))phenylmethylene-κC(α)]phenyl]chromium]pyridine-κN]manganese(I)

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Chemical Name:tricarbonyl[2-[tricarbonyl[η(6)-2[(phenyl-κ(2)C(1')C(2'))phenylmethylene-κC(α)]phenyl]chromium]pyridine-κN]manganese(I)
CAS No.:321424-43-5
Molecular Formula:C₃₀H₂₂CrMnNO₇
Molecular Weight:615.441
Hs Code.:

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Chemical Property of tricarbonyl[2-[tricarbonyl[η(6)-2[(phenyl-κ(2)C(1')C(2'))phenylmethylene-κC(α)]phenyl]chromium]pyridine-κN]manganese(I)

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Technology Process of tricarbonyl[2-[tricarbonyl[η(6)-2[(phenyl-κ(2)C(1')C(2'))phenylmethylene-κC(α)]phenyl]chromium]pyridine-κN]manganese(I)

There total 1 articles about tricarbonyl[2-[tricarbonyl[η(6)-2[(phenyl-κ(2)C(1')C(2'))phenylmethylene-κC(α)]phenyl]chromium]pyridine-κN]manganese(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 321424-35-5
tetracarbonyl[4,4-dimethyl-2-[tricarbonyl(η(6)-phenyl-κC(2'))chromium]-2-oxazoline-κN]manganese(I)

: 908093-98-1
diazodiphenylmethane

: 321424-43-5
tricarbonyl[2-[tricarbonyl[η(6)-2[(phenyl-κ(2)C(1')C(2'))phenylmethylene-κC(α)]phenyl]chromium]pyridine-κN]manganese(I)

Guidance literature:: In n-heptane; 3 equiv. of N2CPh2 and Cr-complex were dissolved in heptane under Ar, mixt. was refluxed for 1 h, additional N2CPh2 was added, suspn. was refluxed for 30 min, mixt. was cooled to room temp.; solvent was removed under vac., residue was dissolved in CH2Cl2, silica was added, solvent was evapd. under vac., residue was dissolved in hexane and chromd. on silica with hexane:CH2Cl2 (5:5), elem. anal.;
DOI:10.1021/om0006920