3,17β-bis(1-ethoxyethoxy)-11β-(4-methylbenzenesulphonyloxymethyl)-oestra-1,3,5(10)-triene

Base Information

Chemical Name:3,17β-bis(1-ethoxyethoxy)-11β-(4-methylbenzenesulphonyloxymethyl)-oestra-1,3,5(10)-triene
CAS No.:76389-94-1
Molecular Formula:C₃₄H₄₈O₇S
Molecular Weight:600.817
Hs Code.:

Synonyms:

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Chemical Property of 3,17β-bis(1-ethoxyethoxy)-11β-(4-methylbenzenesulphonyloxymethyl)-oestra-1,3,5(10)-triene

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Technology Process of 3,17β-bis(1-ethoxyethoxy)-11β-(4-methylbenzenesulphonyloxymethyl)-oestra-1,3,5(10)-triene

There total 4 articles about 3,17β-bis(1-ethoxyethoxy)-11β-(4-methylbenzenesulphonyloxymethyl)-oestra-1,3,5(10)-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76389-88-3
3-hydroxy-11-methyleneoestra-1,3,5⁽¹⁰⁾-trien-17-one

: 76389-94-1
3,17β-bis(1-ethoxyethoxy)-11β-(4-methylbenzenesulphonyloxymethyl)-oestra-1,3,5(10)-triene

Guidance literature:: Multi-step reaction with 4 steps

1: 5.0 g / sodium borohydride / ethanol; tetrahydrofuran; H₂O / 1 h

2: 7.5 g / 4-methylbenzenesulphonyl acid hydrate / 0.75 h / 15 - 20 °C

3: 1.) diborane/dimethylsulphide, 2.) 96 percent ethanol, 3 M sodium hydroxide, 30 percent hydrogen peroxide / 1.) tetrahydrofuran, 3 h, room temperature, 2.) tetrahydrofuran

4: 11 g / pyridine / 1.) 0 deg C, 15 min, 2.) room temperature

With pyridine; sodium hydroxide; sodium tetrahydroborate; dimethylsulfide; ethanol; dihydrogen peroxide; toluene-4-sulfonic acid; diborane; In tetrahydrofuran; ethanol; water;

Reference yield:

: 76389-90-7
3,17β-bis-(1-ethoxyethoxy)-11-methyleneoestra-1,3,5(10)-triene

: 76389-94-1
3,17β-bis(1-ethoxyethoxy)-11β-(4-methylbenzenesulphonyloxymethyl)-oestra-1,3,5(10)-triene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) diborane/dimethylsulphide, 2.) 96 percent ethanol, 3 M sodium hydroxide, 30 percent hydrogen peroxide / 1.) tetrahydrofuran, 3 h, room temperature, 2.) tetrahydrofuran

2: 11 g / pyridine / 1.) 0 deg C, 15 min, 2.) room temperature

With pyridine; sodium hydroxide; dimethylsulfide; ethanol; dihydrogen peroxide; diborane;

Reference yield:

: 76389-89-4
11-methyleneoestra-1,3,5(10)-triene-3,17β-diol

: 76389-94-1
3,17β-bis(1-ethoxyethoxy)-11β-(4-methylbenzenesulphonyloxymethyl)-oestra-1,3,5(10)-triene

Guidance literature:: Multi-step reaction with 3 steps

1: 7.5 g / 4-methylbenzenesulphonyl acid hydrate / 0.75 h / 15 - 20 °C

2: 1.) diborane/dimethylsulphide, 2.) 96 percent ethanol, 3 M sodium hydroxide, 30 percent hydrogen peroxide / 1.) tetrahydrofuran, 3 h, room temperature, 2.) tetrahydrofuran

3: 11 g / pyridine / 1.) 0 deg C, 15 min, 2.) room temperature

With pyridine; sodium hydroxide; dimethylsulfide; ethanol; dihydrogen peroxide; toluene-4-sulfonic acid; diborane;