Technology Process of C28H31(2)H3O6S
There total 4 articles about C28H31(2)H3O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.1 g / lithium aluminium hydride / diethyl ether
2: pyridine, phosphoryl chloride / 48 h / Ambient temperature
3: 1.) (2H6)diborane, 2.) 2 N aq. NaOH, 30percent aq. H2O2 / 1.) THF, diglyme, 2.) THF, diglyme, ethanol, reflux, 1 h
4: 766 mg / pyridine / 240 h / Ambient temperature
With
pyridine; sodium hydroxide; lithium aluminium tetrahydride; diborane-d6; dihydrogen peroxide; trichlorophosphate;
In
diethyl ether;
DOI:10.1071/CH9830403
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) (2H6)diborane, 2.) 2 N aq. NaOH, 30percent aq. H2O2 / 1.) THF, diglyme, 2.) THF, diglyme, ethanol, reflux, 1 h
2: 766 mg / pyridine / 240 h / Ambient temperature
With
pyridine; sodium hydroxide; diborane-d6; dihydrogen peroxide;
DOI:10.1071/CH9830403
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine, phosphoryl chloride / 48 h / Ambient temperature
2: 1.) (2H6)diborane, 2.) 2 N aq. NaOH, 30percent aq. H2O2 / 1.) THF, diglyme, 2.) THF, diglyme, ethanol, reflux, 1 h
3: 766 mg / pyridine / 240 h / Ambient temperature
With
pyridine; sodium hydroxide; diborane-d6; dihydrogen peroxide; trichlorophosphate;
DOI:10.1071/CH9830403
