4-Phenyl-bicyclo <2.2.2> octan-2-ol

Base Information

Chemical Name:4-Phenyl-bicyclo <2.2.2> octan-2-ol
CAS No.:58143-95-6
Molecular Formula:C₁₄H₁₈O
Molecular Weight:202.296
Hs Code.:

Synonyms:

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Chemical Property of 4-Phenyl-bicyclo <2.2.2> octan-2-ol

Chemical Property:

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Technology Process of 4-Phenyl-bicyclo <2.2.2> octan-2-ol

There total 10 articles about 4-Phenyl-bicyclo <2.2.2> octan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58143-66-1,58143-67-2
2-Phenylhex-4-en-al

: 58143-95-6
4-Phenyl-bicyclo <2.2.2> octan-2-ol

Guidance literature:: Multi-step reaction with 8 steps

1: (i) pyrrolidine, (ii) /BRN= 506021/, (iii) aq. AcOH

2: LiAlH₄

3: H₂SO₄

4: iBu₂AlH

5: CrO₃, Ac₂O

6: H₂ / Pd-C

7: MCPBA

8: LiAlH₄

With chromium(VI) oxide; lithium aluminium tetrahydride; sulfuric acid; hydrogen; acetic anhydride; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal;
DOI:10.1002/hlca.19750580517

Reference yield:

: 105909-60-2
2-phenyl-hex-4-enenitrile

: 58143-95-6
4-Phenyl-bicyclo <2.2.2> octan-2-ol

Guidance literature:: Multi-step reaction with 9 steps

1: iBu₂AlH

2: (i) pyrrolidine, (ii) /BRN= 506021/, (iii) aq. AcOH

3: LiAlH₄

4: H₂SO₄

5: iBu₂AlH

6: CrO₃, Ac₂O

7: H₂ / Pd-C

8: MCPBA

9: LiAlH₄

With chromium(VI) oxide; lithium aluminium tetrahydride; sulfuric acid; hydrogen; acetic anhydride; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal;
DOI:10.1002/hlca.19750580517

Reference yield:

: 140-29-4
phenylacetonitrile

: 58143-95-6
4-Phenyl-bicyclo <2.2.2> octan-2-ol

Guidance literature:: Multi-step reaction with 10 steps

1: aq. NaOH, 2NEt₃>Cl

2: iBu₂AlH

3: (i) pyrrolidine, (ii) /BRN= 506021/, (iii) aq. AcOH

4: LiAlH₄

5: H₂SO₄

6: iBu₂AlH

7: CrO₃, Ac₂O

8: H₂ / Pd-C

9: MCPBA

10: LiAlH₄

With chromium(VI) oxide; sodium hydroxide; lithium aluminium tetrahydride; sulfuric acid; N-benzyl-N,N,N-triethylammonium chloride; hydrogen; acetic anhydride; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal;
DOI:10.1002/hlca.19750580517