Technology Process of C26H21NO4
There total 5 articles about C26H21NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
ethanol;
at 0 - 20 ℃;
DOI:10.1002/chem.201102802
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 2 h / -40 °C / Inert atmosphere
1.2: -40 - 20 °C / Inert atmosphere
2.1: ammonium chloride / tetrahydrofuran; water / 2 h / Inert atmosphere
3.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / 1,4-dioxane / 12 h / 100 °C / Inert atmosphere
4.1: boron trifluoride diethyl etherate / ethanol / 0 - 20 °C
With
tetrakis(triphenylphosphine) palladium(0); boron trifluoride diethyl etherate; isopropylmagnesium chloride; ammonium chloride; caesium carbonate;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water;
DOI:10.1002/chem.201102802
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonium chloride / tetrahydrofuran; water / 2 h / Inert atmosphere
2: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / 1,4-dioxane / 12 h / 100 °C / Inert atmosphere
3: boron trifluoride diethyl etherate / ethanol / 0 - 20 °C
With
tetrakis(triphenylphosphine) palladium(0); boron trifluoride diethyl etherate; ammonium chloride; caesium carbonate;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water;
DOI:10.1002/chem.201102802
