3-ETHOXY-AZETIDINE HYDROCHLORIDE

Base Information

• Chemical Name: 3-ETHOXY-AZETIDINE HYDROCHLORIDE
• CAS No.: 535924-73-3
• Molecular Formula: C5H11 N O . Cl H
• Molecular Weight: 137.609
• Hs Code.: 2933990090
• Mol file: 535924-73-3.mol

Synonyms:Azetidine, 3-ethoxy-, hydrochloride (9CI);3-Ethoxyazetidine hydrochloride

Chemical Property of 3-ETHOXY-AZETIDINE HYDROCHLORIDE

Chemical Property:

• PSA: 21.26000
• LogP: 1.12550
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

3-Ethoxyazetidinehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-ETHOXY-AZETIDINE HYDROCHLORIDE

There total 2 articles about 3-ETHOXY-AZETIDINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.1%

tert-butyl 3-ethoxyazetidine-1-carboxylate (1314985-57-3) → 3-ethoxyazetidine hydrochloride (535924-73-3)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; isopropanol; at 20 ℃;

Reference yield:

→ 3-ethoxyazetidine hydrochloride (535924-73-3)

Guidance literature:

Reference yield: 37.0%

3-ethoxyazetidine hydrochloride (535924-73-3) + 5-[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]-3-methyl-2-[methyl(4-oxocyclohexyl)amino]-5,6,7,8-tetrahydro-4H-thieno[3,2-c]azepin-4-one → 5-[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]-2-{[trans-4-(3-ethoxyazetidin-1-yl)cyclohexyl](methyl)amino}-3-methyl-5,6,7,8-tetrahydro-4H-thieno[3,2-c]azepin-4-one

Guidance literature:

3-ethoxyazetidine hydrochloride; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 0.5h;

5-[(4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl]-3-methyl-2-[methyl(4-oxocyclohexyl)amino]-5,6,7,8-tetrahydro-4H-thieno[3,2-c]azepin-4-one; In tetrahydrofuran; methanol; at 20 ℃; for 0.5h;

With lithium borohydride; In tetrahydrofuran; methanol; at -78 - 20 ℃; for 2h;

upstream raw materials:

tert-butyl 3-ethoxyazetidine-1-carboxylate

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