2-{2-[(S)-6-Benzyloxycarbonylamino-2-(2-{2-[(S)-6-benzyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionic acid

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Chemical Name:2-{2-[(S)-6-Benzyloxycarbonylamino-2-(2-{2-[(S)-6-benzyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionic acid
CAS No.:205756-76-9
Molecular Formula:C₅₉H₇₆N₈O₁₃
Molecular Weight:1105.3
Hs Code.:

2-{2-[(S)-6-Benzyloxycarbonylamino-2-(2-{2-[(S)-6-benzyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionic acid

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Chemical Property of 2-{2-[(S)-6-Benzyloxycarbonylamino-2-(2-{2-[(S)-6-benzyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionic acid

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

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Useful:

Technology Process of 2-{2-[(S)-6-Benzyloxycarbonylamino-2-(2-{2-[(S)-6-benzyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionic acid

There total 4 articles about 2-{2-[(S)-6-Benzyloxycarbonylamino-2-(2-{2-[(S)-6-benzyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83537-95-5
H-Aib-Aib-O(t-Bu)

: 205756-76-9
2-{2-[(S)-6-Benzyloxycarbonylamino-2-(2-{2-[(S)-6-benzyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionic acid

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N'-<3-(dimethylamino)propyl>carbodiimide hydrochloride, 1-hydroxybenzotriazole, N-methylmorpholine

2: diethylamine / catalytic hydrogenolysis

3: N-ethyl-N'-<3-(dimethylamino)propyl>carbodiimide hydrochloride, 1-hydroxy-7-azabenzotriazole

4: trifluoroacetic acid / CH₂Cl₂

With 4-methyl-morpholine; 1-hydroxy-7-aza-benzotriazole; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; trifluoroacetic acid; In dichloromethane;

Reference yield:

: 205756-73-6
2-{2-[(S)-6-Benzyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionic acid tert-butyl ester

: 205756-76-9
2-{2-[(S)-6-Benzyloxycarbonylamino-2-(2-{2-[(S)-6-benzyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: diethylamine / catalytic hydrogenolysis

2: N-ethyl-N'-<3-(dimethylamino)propyl>carbodiimide hydrochloride, 1-hydroxy-7-azabenzotriazole

3: trifluoroacetic acid / CH₂Cl₂

With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; trifluoroacetic acid; In dichloromethane;

Reference yield:

: 205756-74-7
2-{2-[(S)-6-Benzyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionic acid

: 205756-76-9
2-{2-[(S)-6-Benzyloxycarbonylamino-2-(2-{2-[(S)-6-benzyloxycarbonylamino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionylamino)-hexanoylamino]-2-methyl-propionylamino}-2-methyl-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N'-<3-(dimethylamino)propyl>carbodiimide hydrochloride, 1-hydroxy-7-azabenzotriazole

2: trifluoroacetic acid / CH₂Cl₂

With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;