N-benzylcatharanthine

Base Information

Chemical Name:N-benzylcatharanthine
CAS No.:83113-28-4
Molecular Formula:C₂₈H₃₀N₂O₂
Molecular Weight:426.558
Hs Code.:

Synonyms:

Suppliers and Price of N-benzylcatharanthine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzylcatharanthine

Chemical Property:

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Technology Process of N-benzylcatharanthine

There total 8 articles about N-benzylcatharanthine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 100-44-7
benzyl chloride

: 2645-61-6
catharanthine hydrochloride

: 83113-28-4
N-benzylcatharanthine

Guidance literature:: With potassium hydride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; 1.) -23 degC, 2.) 70 degC, 5 h;
DOI:10.1139/v82-187

Reference yield:

: 56895-60-4
2-(2-methyl-1H-indol-3-yl)ethanol

: 83113-28-4
N-benzylcatharanthine

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / potassium hydride / diethyl ether; hexamethylphosphoric acid triamide / 2.5 h / Ambient temperature

2: 91 percent / N-bromosuccinimide / benzene / 2 h / 0 °C

3: 33 percent / potassium cyanide / methanol / 24 h / Heating

4: 1.)0 degC, 1 h, 2.) 55 degC, 72 h

5: 18 h / 50 °C

With potassium cyanide; N-Bromosuccinimide; potassium hydride; In methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; benzene;
DOI:10.1139/v82-187

Reference yield:

: 83087-79-0
N,O-dibenzyl-2-methyltryptophol

: 83113-28-4
N-benzylcatharanthine

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / N-bromosuccinimide / benzene / 2 h / 0 °C

2: 33 percent / potassium cyanide / methanol / 24 h / Heating

3: 1.)0 degC, 1 h, 2.) 55 degC, 72 h

4: 18 h / 50 °C

With potassium cyanide; N-Bromosuccinimide; In methanol; benzene;
DOI:10.1139/v82-187