Phccc, (+)-

Base Information

Chemical Name:Phccc, (+)-
CAS No.:177610-87-6
Molecular Formula:C₁₇H₁₄N₂O₃
Molecular Weight:294.31
Hs Code.:
UNII:875PGG7NBA,8JWN87FEQ8
Mol file:177610-87-6.mol

Synonyms:Phccc, (+)-;875PGG7NBA;8JWN87FEQ8;7,7a-Dihydro-7-(hydroxyimino)-N-phenylbenzo(b)cyclopropa(E)pyran-1a(1H)-carboxamide;Benzo(b)cyclopropa(E)pyran-1a(1H)-carboxamide, 7,7a-dihydro-7-(hydroxyimino)-N-phenyl-;1884230-22-1;Benzo(b)cyclopropa(E)pyran-1a(1H)-carboxamide, 7,7a-dihydro-7-(hydroxyimino)-N-phenyl-, (1aR,7E,7aR)-;Benzo(b)cyclopropa(E)pyran-1a(1H)-carboxamide, 7,7a-dihydro-7-(hydroxyimino)-N-phenyl-, (E)-;UNII-875PGG7NBA;UNII-8JWN87FEQ8;VU0359869-3

Suppliers and Price of Phccc, (+)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Phccc, (+)-

Chemical Property:

Boiling Point:579.1±50.0 °C(Predicted)
PKA:10.79±0.40(Predicted)
PSA：70.92000
Density:1.41±0.1 g/cm3(Predicted)
LogP:2.72770
XLogP3:2.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:294.10044231
Heavy Atom Count:22
Complexity:486

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C2C1(OC3=CC=CC=C3C2=NO)C(=O)NC4=CC=CC=C4
Isomeric SMILES:C1[C@H]\2[C@@]1(OC3=CC=CC=C3/C2=N/O)C(=O)NC4=CC=CC=C4

Technology Process of Phccc, (+)-

There total 2 articles about Phccc, (+)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 2-Oxo-1a,2-dihydro-1H-7-oxa-cyclopropa[b]naphthalene-7a-carboxylic acid phenylamide

: 177610-87-6,179068-02-1
PHCCC

Guidance literature:: With hydroxylamine hydrochloride; In tetrahydrofuran; at 80 ℃;
DOI:10.1016/0960-894X(96)00104-7

Reference yield:

: 3845-16-7
N-Phenyl-4(H)-oxo-1-benzopyran-2-carboxamide

: 177610-87-6,179068-02-1
PHCCC

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / NaOH / dimethylformamide / 50 °C

2: 86 percent / NH₂OH*HCl / tetrahydrofuran / 80 °C

With sodium hydroxide; hydroxylamine hydrochloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/0960-894X(96)00104-7