(+/-)-5-<2--N-methylamino>propyl>-2-methoxybenzenesulfonamide

Base Information

Chemical Name:(+/-)-5-<2--N-methylamino>propyl>-2-methoxybenzenesulfonamide
CAS No.:144818-58-6
Molecular Formula:C₂₀H₂₇FN₂O₅S
Molecular Weight:426.509
Hs Code.:

(+/-)-5-<2-<N-<2-(5-fluoro-2-methoxyphenoxy)ethyl>-N-methylamino>propyl>-2-methoxybenzenesulfonamide

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-5-<2--N-methylamino>propyl>-2-methoxybenzenesulfonamide

Chemical Property:

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Technology Process of (+/-)-5-<2--N-methylamino>propyl>-2-methoxybenzenesulfonamide

There total 6 articles about (+/-)-5-<2--N-methylamino>propyl>-2-methoxybenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-(2-{[2-(5-Fluoro-2-methoxy-phenoxy)-ethyl]-formyl-amino}-propyl)-2-methoxy-benzenesulfonamide

: 144818-58-6
(+/-)-5-<2--N-methylamino>propyl>-2-methoxybenzenesulfonamide

Guidance literature:: With sodium tetrahydroborate; In methanol; water; for 1h; Yield given; Ambient temperature;
DOI:10.1248/cpb.40.1443

Reference yield:

: 122-84-9
4-methoxybenzyl methyl ketone

: 144818-58-6
(+/-)-5-<2--N-methylamino>propyl>-2-methoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1: 11.4 g / ClSO₃H / 2 h / Ambient temperature

2: conc. aq. NH₄OH / tetrahydrofuran / 2 h / Ambient temperature

3: methanol / 1 h / Heating

4: NaBH₄ / methanol / 3 h / Ambient temperature

5: methanol; H₂O / 1 h / Heating

6: NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

With chlorosulfonic acid; ammonium hydroxide; sodium tetrahydroborate; In tetrahydrofuran; methanol; water;
DOI:10.1248/cpb.40.1443

Reference yield:

: 116091-63-5
2-methoxy-5-(2-oxopropyl)benzenesulfonamide

: 144818-58-6
(+/-)-5-<2--N-methylamino>propyl>-2-methoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: methanol / 1 h / Heating

2: NaBH₄ / methanol / 3 h / Ambient temperature

3: methanol; H₂O / 1 h / Heating

4: NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

With sodium tetrahydroborate; In methanol; water;
DOI:10.1248/cpb.40.1443