2-hydroxy-4,6-diphenyl-thiobenzophenone

Base Information

• Chemical Name: 2-hydroxy-4,6-diphenyl-thiobenzophenone
• CAS No.: 118428-73-2
• Molecular Formula: C₂₅H₁₈OS
• Molecular Weight: 366.483
• Mol file: 118428-73-2.mol

Synonyms:

Chemical Property of 2-hydroxy-4,6-diphenyl-thiobenzophenone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-hydroxy-4,6-diphenyl-thiobenzophenone

There total 2 articles about 2-hydroxy-4,6-diphenyl-thiobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Acetoxy-4,6-diphenyl-thiobenzophenon (118428-66-3) → 2-hydroxy-4,6-diphenyl-thiobenzophenone (118428-73-2)

Guidance literature:

With hydrogenchloride; In ethanol; water; acetone; for 2.5h; Yield given; Heating;

Reference yield:

2,4,6-triphenylthiopyrylium perchlorate (2930-37-2) → 2-hydroxy-4,6-diphenyl-thiobenzophenone (118428-73-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 29 percent / sodium acetate / 6 h / Heating; other condensing agents

2: conc. HCl / H₂O; ethanol; acetone / 2.5 h / Heating

With hydrogenchloride; sodium acetate; In ethanol; water; acetone;

Reference yield: 82.0%

nickel(II) acetate tetrahydrate (6018-89-9) + 2-hydroxy-4,6-diphenyl-thiobenzophenone (118428-73-2) → Ni(C6H5C(S)(C6H5)2C6H2O)2 (152577-98-5)

Guidance literature:

In methanol; water; acetone; to a soln. of ligand in acetone a soln. of nickel acetate*4H2O in a mixt. of water/methanol is added; ppt. is filtered off, boiled off in acetone and recrystd. from chloroform/ethanol, elem. anal.;

upstream raw materials:

2-Acetoxy-4,6-diphenyl-thiobenzophenon

2,4,6-triphenylthiopyrylium perchlorate

Downstream raw materials:

2-Hydroxy-4,6-diphenyl-benzophenon

Ni(C₆H₅C(S)(C₆H₅)2C₆H₂O)2

Co(C₆H₅C(S)(C₆H₅)2C₆H₂O)3