1,2-C₆F₄(B(C(C₆F₅)2)2*MeCN

Base Information

• Chemical Name: 1,2-C₆F₄(B(C(C₆F₅)2)2*MeCN
• CAS No.: 874395-51-4
• Molecular Formula: C₃₂H₃B₂F₂₄N
• Molecular Weight: 878.966
• Mol file: 874395-51-4.mol

Synonyms:

Chemical Property of 1,2-C₆F₄(B(C(C₆F₅)2)2*MeCN

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,2-C₆F₄(B(C(C₆F₅)2)2*MeCN

There total 1 articles about 1,2-C₆F₄(B(C(C₆F₅)2)2*MeCN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

acetonitrile (75-05-8,26809-02-9) + 1,2-C6F4(B(C(C6F5)2)2 (223769-13-9) → 1,2-C6F4(B(C(C6F5)2)2*MeCN (874395-51-4)

Guidance literature:

In dichloromethane; acetonitrile; (N2); Schlenk technique; MeCN was added to soln. of B compd. in CH2Cl2; mixt. was stirred for 1 h; volatiles removed (vac.);

DOI:10.1021/om050764t

Reference yield:

o-C6F4(1,2,3,4,5,6,7,8-octafluoro-9-borafluorene)2 (784170-27-0) + 1,2-C6F4(B(C(C6F5)2)2*MeCN (874395-51-4) → 1,2-C6F4(B(C12F8))2*MeCN (874395-53-6) + 1,2-C6F4(B(C(C6F5)2)2 (223769-13-9)

Guidance literature:

In not given; NMR monitoring;

DOI:10.1021/om050764t

upstream raw materials:

acetonitrile

1,2-C₆F₄(B(C(C₆F₅)2)2

Downstream raw materials:

1,2-C₆F₄(B(C₁₂F₈))2*MeCN

1,2-C₆F₄(B(C(C₆F₅)2)2