C₃₅H₄₄O₇

Base Information

Chemical Name:C₃₅H₄₄O₇
CAS No.:72065-03-3
Molecular Formula:C₃₅H₄₄O₇
Molecular Weight:576.73
Hs Code.:

C<sub>35</sub>H<sub>44</sub>O<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₅H₄₄O₇

Chemical Property:

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Technology Process of C₃₅H₄₄O₇

There total 8 articles about C₃₅H₄₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.8%

: 72065-01-1
15-deoxy-15-oxo-11-epi-PGF_2α

: 72065-03-3
C₃₅H₄₄O₇

: 72065-02-2
11-epi-PGF_2α-methyl ester 9,11-dibenzoate

Guidance literature:: With zinc borohydride; In 1,2-dimethoxyethane; diethyl ether; Ambient temperature;
DOI:10.1248/cpb.31.2607

Reference yield:

: 72064-92-7
methyl (Z)-7-<(1R,2R,3R,5S)-5-tert-butyldimethylsilyloxy-2-<(tetrahydro-2-pyranyloxy)metyl>-3-hydroxycyclopentyl>-5-heptenoate

: 72065-03-3
C₃₅H₄₄O₇

Guidance literature:: Multi-step reaction with 7 steps

1: 195 mg / Et₃N / CH₂Cl₂ / 0.5 h / -25 °C

2: 1.) 18-crown-6/KO₂ / 1.) DMSO/DME, rt, 7 h; 2.) ether, 0 deg C

3: 100 mg / pyridine / CH₂Cl₂ / 2 h / Ambient temperature

4: AcOH / H₂O; tetrahydrofuran / 12 h / 45 °C

5: CrO₃*2pyridine, celite-545 / CH₂Cl₂ / 1 h

6: NaH / 1,2-dimethoxy-ethane / 2 h / Ambient temperature

7: zinc borohydride / diethyl ether; 1,2-dimethoxy-ethane / Ambient temperature

With pyridine; 18-crown-6 ether; Celite; zinc borohydride; dipyridine chromium trioxide; sodium hydride; acetic acid; triethylamine; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water;
DOI:10.1248/cpb.31.2607

Reference yield:

: 72064-97-2
methyl (Z)-7-<(1R,2R,3R,5S)-5-tert-butyldimethylsilyloxy-2-<(tetrahydro-2-pyranyloxy)metyl>-3-methylsulfonyloxycyclopentyl>-5-heptenoate

: 72065-03-3
C₃₅H₄₄O₇

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) 18-crown-6/KO₂ / 1.) DMSO/DME, rt, 7 h; 2.) ether, 0 deg C

2: 100 mg / pyridine / CH₂Cl₂ / 2 h / Ambient temperature

3: AcOH / H₂O; tetrahydrofuran / 12 h / 45 °C

4: CrO₃*2pyridine, celite-545 / CH₂Cl₂ / 1 h

5: NaH / 1,2-dimethoxy-ethane / 2 h / Ambient temperature

6: zinc borohydride / diethyl ether; 1,2-dimethoxy-ethane / Ambient temperature

With pyridine; 18-crown-6 ether; Celite; zinc borohydride; dipyridine chromium trioxide; sodium hydride; acetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water;
DOI:10.1248/cpb.31.2607