3-(3,5-Di-tert-butylphenyl)propionic acid, 96%

Base Information

• Chemical Name: 3-(3,5-Di-tert-butylphenyl)propionic acid, 96%
• CAS No.: 42288-01-7
• Molecular Formula: C17H26 O2
• Molecular Weight: 262.38700
• Mol file: 42288-01-7.mol

Synonyms:3,5-Di-tert-butylhydrocinnamicacid; Hydrocinnamic acid, 3,5-di-tert-butyl-

Chemical Property of 3-(3,5-Di-tert-butylphenyl)propionic acid, 96%

Chemical Property:

• Melting Point: 103-108℃
• PSA: 37.30000
• LogP: 4.29880

Purity/Quality:

99% ^*data from raw suppliers

3-(3,5-Di-tert-butylphenyl)propionic acid, 96% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(3,5-Di-tert-butylphenyl)propionic acid, 96%

There total 1 articles about 3-(3,5-Di-tert-butylphenyl)propionic acid, 96% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-di-t-butylcinnamic acid (180969-07-7) → 3-(3,5-di-tert-butylphenyl)propanoic acid (42288-01-7)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.bmc.2009.04.010

Reference yield: 88.0%

3-(3,5-di-tert-butylphenyl)propanoic acid (42288-01-7) + (3-fluoro-4-(methylsulfonamido)phenyl)methanaminium chloride → 3-(3,5-di-tert-butylphenyl)-N-(3-fluoro-4-(methylsulfonamido)benzyl)propanamide (1165738-63-5)

Guidance literature:

3-(3,5-di-tert-butylphenyl)propanoic acid; With 4-methyl-morpholine; triethylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In tetrahydrofuran; for 4h;

(3-fluoro-4-(methylsulfonamido)phenyl)methanaminium chloride; In tetrahydrofuran; at 20 ℃; for 10h;

DOI:10.1016/j.bmc.2009.04.010

Reference yield:

3-(3,5-di-tert-butylphenyl)propanoic acid (42288-01-7) → 2-(3,5-Di-tert-butyl-phenyl)-ethylamine; hydrochloride (140401-63-4)

Guidance literature:

With hydrogenchloride; sodium azide; Multistep reaction; 2) ether;

DOI:10.1002/recl.19921110103

upstream raw materials:

3,5-di-t-butylcinnamic acid

Downstream raw materials:

2-(3,5-Di-tert-butyl-phenyl)-ethylamine; hydrochloride

3-(3,5-di-tert-butylphenyl)-N-(3-fluoro-4-(methylsulfonamido)benzyl)propanamide

Refernces