[CuBr(N-carboethoxy-4-bromobenzene thioamide)(AsPh₃)2]

Base Information

• Chemical Name: [CuBr(N-carboethoxy-4-bromobenzene thioamide)(AsPh₃)2]
• CAS No.: 505058-76-4
• Molecular Formula: C₄₆H₄₀As₂Br₂CuNO₂S
• Molecular Weight: 1044.09
• Mol file: 505058-76-4.mol

Synonyms:

Chemical Property of [CuBr(N-carboethoxy-4-bromobenzene thioamide)(AsPh₃)2]

Chemical Property:

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Technology Process of [CuBr(N-carboethoxy-4-bromobenzene thioamide)(AsPh₃)2]

There total 1 articles about [CuBr(N-carboethoxy-4-bromobenzene thioamide)(AsPh₃)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

tris(triphenylarsine)copper(I) bromide (33634-30-9) + ethyl N-(4-bromobenzenecarbothioyl)carbamate (57774-75-1) → [CuBr(N-carboethoxy-4-bromobenzene thioamide)(AsPh3)2] (505058-76-4)

Guidance literature:

In benzene; byproducts: AsPh3; soln. N-carboethoxy-4-bromobenzene thioamide (benzene), soln. CuBr(AsPh3)3 (benzene); mixed at 25°C; heated under reflux for 0.5 to 1 h; concd. to half volume under reduced pressure; addition of petroleum ether (60-80°C); stand for 2-3 h; filtered;washed several times (petroleum ether); dried in vac.; elem. anal.;

DOI:10.1081/SIM-120016465

upstream raw materials:

tris(triphenylarsine)copper(I) bromide

ethyl N-(4-bromobenzenecarbothioyl)carbamate