[Cu₂(phenyl 2-pyridyl ketone oxime^(1-))2(hexafluoroacetylacetonate)2]

Base Information

• Chemical Name: [Cu₂(phenyl 2-pyridyl ketone oxime^(1-))2(hexafluoroacetylacetonate)2]
• CAS No.: 1211004-20-4
• Molecular Formula: C₃₄H₂₀Cu₂F₁₂N₄O₆
• Molecular Weight: 935.629

Synonyms:

Chemical Property of [Cu₂(phenyl 2-pyridyl ketone oxime^(1-))2(hexafluoroacetylacetonate)2]

Chemical Property:

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Technology Process of [Cu₂(phenyl 2-pyridyl ketone oxime^(1-))2(hexafluoroacetylacetonate)2]

There total 1 articles about [Cu₂(phenyl 2-pyridyl ketone oxime^(1-))2(hexafluoroacetylacetonate)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

copper(II) choride dihydrate + hexafluoroacetylacetone sodium salt + phenyl-2-pyridyl ketoxime (1826-28-4) → [Cu2(phenyl 2-pyridyl ketone oxime(1-))2(hexafluoroacetylacetonate)2] (1211004-20-4)

Guidance literature:

In dichloromethane; CuCl2 added to CH2Cl2 soln. of phenyl 2-pyridyl ketone oxime, sodium hexafluoroacetylacetonate; stirred for 40 min; filtered; layered with Et2O/hexane (1:1, v/v); crystd. after 3 d; filtered; washed twice with CH2Cl2, twice with Et2O; air dried; elem. anal.;

DOI:10.1016/j.poly.2009.07.010

upstream raw materials:

phenyl-2-pyridyl ketoxime

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