tetraphenylphosphonium dioxotribromoruthenate(VI)

Base Information

Chemical Name:tetraphenylphosphonium dioxotribromoruthenate(VI)
CAS No.:131382-88-2
Molecular Formula:Br₃O₂Ru*C₂₄H₂₀P
Molecular Weight:712.177
Hs Code.:

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Chemical Property of tetraphenylphosphonium dioxotribromoruthenate(VI)

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Technology Process of tetraphenylphosphonium dioxotribromoruthenate(VI)

There total 1 articles about tetraphenylphosphonium dioxotribromoruthenate(VI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20427-56-9
ruthenium tetroxide

: 24038-30-0
tetraphenylphosphonium bromide

: 131382-88-2
tetraphenylphosphonium dioxotribromoruthenate(VI)

Guidance literature:: With hydrogen bromide; In tetrachloromethane; sodium hydroxide; RuO4 (generated from RuO2*nH2O, NaIO4 and water) passed into CCl4 (N2 gas stream), yellow soln. stirred overnight with 2.5M NaOH soln., aq. layer contg. trans-(RuO3(OH)2)(2-) separated, cooled (0°C), Ph4PBr added, then HBr dropwise, pptn.; solid filtered off, washed (cold water), dried (vac.), elem. anal.;
DOI:10.1016/S0277-5387(00)83983-2

Reference yield:

: 131382-88-2
tetraphenylphosphonium dioxotribromoruthenate(VI)

: tetraphenylphosphonium dioxotetrabromoruthenate(VI)

Guidance literature:: In tetrachloromethane; dichloromethane; Ru-complex dissolved in CH2Cl2 and CCl4 (10:1), green soln. reduced in vol. until red; crystn. (room temp., overnight), filtered, washed (cold water), dried (dessicator, silica gel), elem. anal.;
DOI:10.1016/S0277-5387(00)83983-2