8-Heptadecen-2-ol, 2-acetate, (2R,8Z)-

Base Information

Chemical Name:8-Heptadecen-2-ol, 2-acetate, (2R,8Z)-
CAS No.:1199746-71-8
Molecular Formula:C₁₉H₃₆O₂
Molecular Weight:296.494
Hs Code.:
Mol file:1199746-71-8.mol

Synonyms:

Suppliers and Price of 8-Heptadecen-2-ol, 2-acetate, (2R,8Z)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-Heptadecen-2-ol, 2-acetate, (2R,8Z)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 8-Heptadecen-2-ol, 2-acetate, (2R,8Z)-

There total 9 articles about 8-Heptadecen-2-ol, 2-acetate, (2R,8Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 764-93-2
1-decyne

: 1199746-71-8
(1R,7Z)-1-methyl-7-hexadecenyl acetate

: (1R,7E)-1-methyl-7-hexadecenyl acetate

: 56599-51-0
(1R)-1-methyl-7-hexadecenyl acetate

Guidance literature:: Multi-step reaction with 6 steps

1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

3: [(S,S)-N,N’-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(II); water; toluene-4-sulfonic acid / dichloromethane / 20 °C / Resolution of racemate

4: lithium aluminium tetrahydride / diethyl ether

5: hydrogen / cyclohexane / 2 h / 20 °C / 760.05 Torr

6: pyridine

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; [(S,S)-N,N’-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(II); n-butyllithium; water; hydrogen; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; cyclohexane;
DOI:10.1271/bbb.120265

Reference yield:

: 1392275-19-2
1-heptadecen-8-yne

: 1199746-71-8
(1R,7Z)-1-methyl-7-hexadecenyl acetate

: (1R,7E)-1-methyl-7-hexadecenyl acetate

: 56599-51-0
(1R)-1-methyl-7-hexadecenyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

2: [(S,S)-N,N’-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(II); water; toluene-4-sulfonic acid / dichloromethane / 20 °C / Resolution of racemate

3: lithium aluminium tetrahydride / diethyl ether

4: hydrogen / cyclohexane / 2 h / 20 °C / 760.05 Torr

5: pyridine

With pyridine; lithium aluminium tetrahydride; [(S,S)-N,N’-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(II); water; hydrogen; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; cyclohexane;
DOI:10.1271/bbb.120265

Reference yield:

: 1392275-20-5
(+/-)-1,2-epoxy-8-heptadecyne

: 1199746-71-8
(1R,7Z)-1-methyl-7-hexadecenyl acetate

: (1R,7E)-1-methyl-7-hexadecenyl acetate

: 56599-51-0
(1R)-1-methyl-7-hexadecenyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: [(S,S)-N,N’-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(II); water; toluene-4-sulfonic acid / dichloromethane / 20 °C / Resolution of racemate

2: lithium aluminium tetrahydride / diethyl ether

3: hydrogen / cyclohexane / 2 h / 20 °C / 760.05 Torr

4: pyridine

With pyridine; lithium aluminium tetrahydride; [(S,S)-N,N’-bis(3,5-di-tertbutylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(II); water; hydrogen; toluene-4-sulfonic acid; In diethyl ether; dichloromethane; cyclohexane;
DOI:10.1271/bbb.120265