γ-benzyl ester of the O-<γ-benzyl ester of (benzyl 2-acetamido-4-O-acetyl-2-deoxy-α-D-glucopyranosid)uronyl-L-alanyl-D-isoglutamin-3-yl>-D-lactoyl-L-alanyl-D-isoglutamine

Base Information

Chemical Name:γ-benzyl ester of the O-<γ-benzyl ester of (benzyl 2-acetamido-4-O-acetyl-2-deoxy-α-D-glucopyranosid)uronyl-L-alanyl-D-isoglutamin-3-yl>-D-lactoyl-L-alanyl-D-isoglutamine
CAS No.:122768-13-2
Molecular Formula:C₅₀H₆₃N₇O₁₆
Molecular Weight:1018.09
Hs Code.:

γ-benzyl ester of the O-<γ-benzyl ester of (benzyl 2-acetamido-4-O-acetyl-2-deoxy-α-D-glucopyranosid)uronyl-L-alanyl-D-isoglutamin-3-yl>-D-lactoyl-L-alanyl-D-isoglutamine

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Chemical Property of γ-benzyl ester of the O-<γ-benzyl ester of (benzyl 2-acetamido-4-O-acetyl-2-deoxy-α-D-glucopyranosid)uronyl-L-alanyl-D-isoglutamin-3-yl>-D-lactoyl-L-alanyl-D-isoglutamine

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Technology Process of γ-benzyl ester of the O-<γ-benzyl ester of (benzyl 2-acetamido-4-O-acetyl-2-deoxy-α-D-glucopyranosid)uronyl-L-alanyl-D-isoglutamin-3-yl>-D-lactoyl-L-alanyl-D-isoglutamine

There total 4 articles about γ-benzyl ester of the O-<γ-benzyl ester of (benzyl 2-acetamido-4-O-acetyl-2-deoxy-α-D-glucopyranosid)uronyl-L-alanyl-D-isoglutamin-3-yl>-D-lactoyl-L-alanyl-D-isoglutamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25605-67-8
benzyl 2-acetamido-4-O-acetyl-3-O--2-deoxy-α-D-glucopyranoside

: 122768-13-2
γ-benzyl ester of the O-<γ-benzyl ester of (benzyl 2-acetamido-4-O-acetyl-2-deoxy-α-D-glucopyranosid)uronyl-L-alanyl-D-isoglutamin-3-yl>-D-lactoyl-L-alanyl-D-isoglutamine

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / CrO₃, 3.5 M aq.H₂SO₄ / acetone / 0 deg C, 15 min, room temperature 2.5 h

2: 0.4 g / H₂ / 10percent Pd-C / tetrahydrofuran / 1 h

3: dicyclohexylcarbodiimid / dioxane; dimethylformamide

4: (C₂H₅)3N / dioxane; dimethylformamide / 48 h

With chromium(VI) oxide; sulfuric acid; hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide; acetone;
DOI:10.1007/BF00598194

Reference yield:

: 121713-53-9
-2-deoxy-α-D-glucopyranosid>uronic acid

: 122768-13-2
γ-benzyl ester of the O-<γ-benzyl ester of (benzyl 2-acetamido-4-O-acetyl-2-deoxy-α-D-glucopyranosid)uronyl-L-alanyl-D-isoglutamin-3-yl>-D-lactoyl-L-alanyl-D-isoglutamine

Guidance literature:: Multi-step reaction with 3 steps

1: 0.4 g / H₂ / 10percent Pd-C / tetrahydrofuran / 1 h

2: dicyclohexylcarbodiimid / dioxane; dimethylformamide

3: (C₂H₅)3N / dioxane; dimethylformamide / 48 h

With hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1007/BF00598194

Reference yield:

: 122748-87-2
benzyl 2-acetamido-4-O-acetyl-3-O-(D-1-carboxyethyl)-2-deoxy-α-D-glucopyranosiduronic acid

: 122768-13-2
γ-benzyl ester of the O-<γ-benzyl ester of (benzyl 2-acetamido-4-O-acetyl-2-deoxy-α-D-glucopyranosid)uronyl-L-alanyl-D-isoglutamin-3-yl>-D-lactoyl-L-alanyl-D-isoglutamine

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexylcarbodiimid / dioxane; dimethylformamide

2: (C₂H₅)3N / dioxane; dimethylformamide / 48 h

With triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1007/BF00598194