[Mn(4-aminoacetophenone semicarbazone)2Cl₂]

Base Information

• Chemical Name: [Mn(4-aminoacetophenone semicarbazone)2Cl₂]
• CAS No.: 864915-90-2
• Molecular Formula: C₁₈H₂₄Cl₂MnN₈O₂
• Molecular Weight: 510.285

Synonyms:

Chemical Property of [Mn(4-aminoacetophenone semicarbazone)2Cl₂]

Chemical Property:

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Technology Process of [Mn(4-aminoacetophenone semicarbazone)2Cl₂]

There total 1 articles about [Mn(4-aminoacetophenone semicarbazone)2Cl₂] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

4-aminoacetophenone semicarbazone + manganese(II) chloride hydrate → [Mn(4-aminoacetophenone semicarbazone)2Cl2] (864915-90-2)

Guidance literature:

In ethanol; water; hot aq. ethanolic soln. salt and hot ethanolic soln. ligand were mixed with constant stirring, mixt. was refluxed for 5 h at 75°C; mixt. was cooled to 5°C, complex was filtered, washed with 50% EtOH, dried over P4O10 under vac., recrystd.; elem. anal.;

DOI:10.1016/j.saa.2004.08.028

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