Phosphoric acid 4-chloro-phenyl ester 2-cyano-ethyl ester (2R,3S,5R)-2-hydroxymethyl-5-[4-(4-methoxy-benzoylamino)-2-oxo-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yl ester

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Chemical Name:Phosphoric acid 4-chloro-phenyl ester 2-cyano-ethyl ester (2R,3S,5R)-2-hydroxymethyl-5-[4-(4-methoxy-benzoylamino)-2-oxo-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yl ester
CAS No.:79715-44-9
Molecular Formula:C₂₆H₂₆ClN₄O₉P
Molecular Weight:604.941
Hs Code.:

Phosphoric acid 4-chloro-phenyl ester 2-cyano-ethyl ester (2R,3S,5R)-2-hydroxymethyl-5-[4-(4-methoxy-benzoylamino)-2-oxo-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yl ester

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Chemical Property of Phosphoric acid 4-chloro-phenyl ester 2-cyano-ethyl ester (2R,3S,5R)-2-hydroxymethyl-5-[4-(4-methoxy-benzoylamino)-2-oxo-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yl ester

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Technology Process of Phosphoric acid 4-chloro-phenyl ester 2-cyano-ethyl ester (2R,3S,5R)-2-hydroxymethyl-5-[4-(4-methoxy-benzoylamino)-2-oxo-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yl ester

There total 4 articles about Phosphoric acid 4-chloro-phenyl ester 2-cyano-ethyl ester (2R,3S,5R)-2-hydroxymethyl-5-[4-(4-methoxy-benzoylamino)-2-oxo-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 80680-41-7
Phosphoric acid 4-chloro-phenyl ester 2-cyano-ethyl ester (2R,3S,5R)-5-[4-(4-methoxy-benzoylamino)-2-oxo-2H-pyrimidin-1-yl]-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester

: 79715-44-9
Phosphoric acid 4-chloro-phenyl ester 2-cyano-ethyl ester (2R,3S,5R)-2-hydroxymethyl-5-[4-(4-methoxy-benzoylamino)-2-oxo-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yl ester

Guidance literature:: With acetic acid; for 4h;
DOI:10.1016/S0040-4039(01)81907-9

Reference yield:

: 99678-42-9
Phosphoric acid 4-chloro-phenyl ester (2R,3S,5R)-5-[4-(4-methoxy-benzoylamino)-2-oxo-2H-pyrimidin-1-yl]-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester

: 79715-44-9
Phosphoric acid 4-chloro-phenyl ester 2-cyano-ethyl ester (2R,3S,5R)-2-hydroxymethyl-5-[4-(4-methoxy-benzoylamino)-2-oxo-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 81 percent / 80percent acetic acid / 4 h

With acetic acid;
DOI:10.1016/S0040-4039(01)81907-9

Reference yield:

: 106-48-9,82344-39-6
4-chloro-phenol

: 79715-44-9
Phosphoric acid 4-chloro-phenyl ester 2-cyano-ethyl ester (2R,3S,5R)-2-hydroxymethyl-5-[4-(4-methoxy-benzoylamino)-2-oxo-2H-pyrimidin-1-yl]-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 5 steps

1: POCl₃

3: triisopropylbenzenesulfonyl chloride / 4 h

5: 81 percent / 80percent acetic acid / 4 h

With triisopropylbenzenesulfonyl chloride; acetic acid; trichlorophosphate;
DOI:10.1016/S0040-4039(01)81907-9