C₅₀H₆₃N₃O₉

Base Information

Chemical Name:C₅₀H₆₃N₃O₉
CAS No.:1255213-75-2
Molecular Formula:C₅₀H₆₃N₃O₉
Molecular Weight:850.065
Hs Code.:

C<sub>50</sub>H<sub>63</sub>N<sub>3</sub>O<sub>9</sub>

Synonyms:

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Chemical Property of C₅₀H₆₃N₃O₉

Chemical Property:

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Technology Process of C₅₀H₆₃N₃O₉

There total 18 articles about C₅₀H₆₃N₃O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1255213-21-8
(S)-methyl 5-nitro-2-(pent-4-en-2-yloxy)benzoate

: 1255213-75-2
C₅₀H₆₃N₃O₉

Guidance literature:: Multi-step reaction with 8 steps

1.1: water; sodium hydroxide / tetrahydrofuran; methanol / 23 h

1.2: pH 1

2.1: thionyl chloride / 2 h / 85 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 0 - 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 0 - 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 14 h / 0 - 20 °C

6.1: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / chlorobenzene / 4 h / 65 °C

7.1: 20% palladium hydroxide on carbon; hydrogen / methanol / 20 °C

8.1: sodium hydrogencarbonate / 1,4-dioxane / 15 h / 0 - 20 °C

With thionyl chloride; Hoveyda-Grubbs catalyst second generation; 20% palladium hydroxide on carbon; tetrabutyl ammonium fluoride; water; hydrogen; sodium hydride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; p-benzoquinone; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; chlorobenzene; mineral oil;
DOI:10.1021/ja105119r

Reference yield:

: 1255213-22-9
C₁₂H₁₃NO₅

: 1255213-75-2
C₅₀H₆₃N₃O₉

Guidance literature:: Multi-step reaction with 7 steps

1: thionyl chloride / 2 h / 85 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 0 - 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 0 - 20 °C

4: sodium hydride / N,N-dimethyl-formamide; mineral oil / 14 h / 0 - 20 °C

5: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / chlorobenzene / 4 h / 65 °C

6: 20% palladium hydroxide on carbon; hydrogen / methanol / 20 °C

7: sodium hydrogencarbonate / 1,4-dioxane / 15 h / 0 - 20 °C

With thionyl chloride; Hoveyda-Grubbs catalyst second generation; 20% palladium hydroxide on carbon; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; chlorobenzene; mineral oil;
DOI:10.1021/ja105119r

Reference yield:

: 1255213-24-1
C₁₂H₁₂ClNO₄

: 1255213-75-2
C₅₀H₆₃N₃O₉

Guidance literature:: Multi-step reaction with 6 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 0 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 0 - 20 °C

3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 14 h / 0 - 20 °C

4: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / chlorobenzene / 4 h / 65 °C

5: 20% palladium hydroxide on carbon; hydrogen / methanol / 20 °C

6: sodium hydrogencarbonate / 1,4-dioxane / 15 h / 0 - 20 °C

With Hoveyda-Grubbs catalyst second generation; 20% palladium hydroxide on carbon; tetrabutyl ammonium fluoride; hydrogen; sodium hydride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; chlorobenzene; mineral oil;
DOI:10.1021/ja105119r