Technology Process of C16H15NO2S
There total 5 articles about C16H15NO2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; sodium acetate;
In
ethanol; water;
at 20 ℃;
for 3.5h;
Inert atmosphere;
DOI:10.1021/ml300050b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / Inert atmosphere
2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 3.5 h / 20 °C / Inert atmosphere
With
hydroxylamine hydrochloride; sodium acetate; pyridinium chlorochromate;
In
ethanol; dichloromethane; water;
DOI:10.1021/ml300050b
- Guidance literature:
-
Multi-step reaction with 5 steps
1: diethyl ether / 1 h / Inert atmosphere; Cooling with ice
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / Inert atmosphere; Cooling with ice
3: thiourea / methanol / 18 h / 20 °C / Inert atmosphere
4: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / Inert atmosphere
5: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 3.5 h / 20 °C / Inert atmosphere
With
hydroxylamine hydrochloride; sodium acetate; thiourea; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate;
In
methanol; diethyl ether; ethanol; dichloromethane; water;
DOI:10.1021/ml300050b