2-(4-Dicyanomethylene-2,3,5,6-tetrafluoro-cyclohexa-2,5-dienylidene)-malononitrile; compound with 1,2-diselena-cyclopenta[cd]fluoranthene

Base Information

Chemical Name:2-(4-Dicyanomethylene-2,3,5,6-tetrafluoro-cyclohexa-2,5-dienylidene)-malononitrile; compound with 1,2-diselena-cyclopenta[cd]fluoranthene
CAS No.:111094-66-7
Molecular Formula:C₁₂F₄N₄*C₁₆H₈Se₂
Molecular Weight:634.312
Hs Code.:

2-(4-Dicyanomethylene-2,3,5,6-tetrafluoro-cyclohexa-2,5-dienylidene)-malononitrile; compound with 1,2-diselena-cyclopenta[cd]fluoranthene

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Chemical Property of 2-(4-Dicyanomethylene-2,3,5,6-tetrafluoro-cyclohexa-2,5-dienylidene)-malononitrile; compound with 1,2-diselena-cyclopenta[cd]fluoranthene

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Technology Process of 2-(4-Dicyanomethylene-2,3,5,6-tetrafluoro-cyclohexa-2,5-dienylidene)-malononitrile; compound with 1,2-diselena-cyclopenta[cd]fluoranthene

There total 7 articles about 2-(4-Dicyanomethylene-2,3,5,6-tetrafluoro-cyclohexa-2,5-dienylidene)-malononitrile; compound with 1,2-diselena-cyclopenta[cd]fluoranthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4208-97-3
5,6-dichloroacenaphthene

: 111094-66-7
2-(4-Dicyanomethylene-2,3,5,6-tetrafluoro-cyclohexa-2,5-dienylidene)-malononitrile; compound with 1,2-diselena-cyclopenta[cd]fluoranthene

Guidance literature:: Multi-step reaction with 6 steps

1: NBS / CCl₄ / Heating

2: Zn / ethanol / Heating

3: 25 percent / toluene / 160 °C / in autoclave

4: 54 percent / chloranil / xylene / Heating

5: 76.6 percent / dimethylformamide

With N-Bromosuccinimide; chloranil; zinc; In tetrachloromethane; ethanol; N,N-dimethyl-formamide; toluene; xylene;
DOI:10.1016/S0040-4039(00)84435-4

Reference yield:

: 83-32-9
acenaphthene

: 111094-66-7
2-(4-Dicyanomethylene-2,3,5,6-tetrafluoro-cyclohexa-2,5-dienylidene)-malononitrile; compound with 1,2-diselena-cyclopenta[cd]fluoranthene

Guidance literature:: Multi-step reaction with 7 steps

1: 52 percent / SO₂Cl₂, anhydrous aluminium chloride / nitrobenzene / 25 - 30 °C

2: NBS / CCl₄ / Heating

3: Zn / ethanol / Heating

4: 25 percent / toluene / 160 °C / in autoclave

5: 54 percent / chloranil / xylene / Heating

6: 76.6 percent / dimethylformamide

With N-Bromosuccinimide; aluminium trichloride; sulfuryl dichloride; chloranil; zinc; In tetrachloromethane; ethanol; nitrobenzene; N,N-dimethyl-formamide; toluene; xylene;
DOI:10.1016/S0040-4039(00)84435-4

Reference yield:

: 33950-95-7
1,2-dibromo-5,6-dichloroacenaphthene

: 111094-66-7
2-(4-Dicyanomethylene-2,3,5,6-tetrafluoro-cyclohexa-2,5-dienylidene)-malononitrile; compound with 1,2-diselena-cyclopenta[cd]fluoranthene

Guidance literature:: Multi-step reaction with 5 steps

1: Zn / ethanol / Heating

2: 25 percent / toluene / 160 °C / in autoclave

3: 54 percent / chloranil / xylene / Heating

4: 76.6 percent / dimethylformamide

With chloranil; zinc; In ethanol; N,N-dimethyl-formamide; toluene; xylene;
DOI:10.1016/S0040-4039(00)84435-4