OsCl(P(C₆H₅)3)2(C₅H₄N)3C₃N₃⁽¹⁺⁾BF₄^(1-)H₂O=OsCl(P(C₆H₅)3)2(C₅H₄N)3C₃N₃BF₄*H₂O

Base Information

Chemical Name:OsCl(P(C₆H₅)3)2(C₅H₄N)3C₃N₃⁽¹⁺⁾*BF₄^(1-)*H₂O=OsCl(P(C₆H₅)3)2(C₅H₄N)3C₃N₃BF₄*H₂O
CAS No.:861393-84-2
Molecular Formula:BF₄*C₅₄H₄₂ClN₆OsP₂*H₂O
Molecular Weight:1167.39
Hs Code.:

OsCl(P(C<sub>6</sub>H<sub>5</sub>)3)2(C<sub>5</sub>H<sub>4</sub>N)3C<sub>3</sub>N<sub>3</sub><sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>*H<sub>2</sub>O=OsCl(P(C<sub>6</sub>H<sub>5</sub>)3)2(C<sub>5</sub>H<sub>4</sub>N)3C<sub>3</sub>N<sub>3</sub>BF<sub>4</sub>*H<sub>2</sub>O

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Chemical Property of OsCl(P(C₆H₅)3)2(C₅H₄N)3C₃N₃⁽¹⁺⁾*BF₄^(1-)*H₂O=OsCl(P(C₆H₅)3)2(C₅H₄N)3C₃N₃BF₄*H₂O

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Technology Process of OsCl(P(C₆H₅)3)2(C₅H₄N)3C₃N₃⁽¹⁺⁾*BF₄^(1-)*H₂O=OsCl(P(C₆H₅)3)2(C₅H₄N)3C₃N₃BF₄*H₂O

There total 1 articles about OsCl(P(C₆H₅)3)2(C₅H₄N)3C₃N₃⁽¹⁺⁾*BF₄^(1-)*H₂O=OsCl(P(C₆H₅)3)2(C₅H₄N)3C₃N₃BF₄*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 13826-83-0
ammonium tetrafluroborate

: diammonium hexachloroosmate(IV)

: 3682-35-7
2,4,6-tris(2-pyridyl)-1,3,5-triazine

: 7732-18-5
water

: 603-35-0
triphenylphosphine

: 861393-84-2
OsCl(P(C₆H₅)3)2(C₅H₄N)3C₃N₃⁽¹⁺⁾*BF₄^(1-)*H₂O=OsCl(P(C₆H₅)3)2(C₅H₄N)3C₃N₃BF₄*H₂O

Guidance literature:: In methanol; a methanolic soln. of Os-complex was added to a refluxing soln. of P(C6H5)3 in methanol, refluxed to 1 h, polypyridyl-compound was added, the mixt. was refluxed for 8-10 h, cooled to room temp.; filtered, reduced in vol., a satd. soln. of NH4BF4 in methanol was added, allowed to stand at 4°C, crystals were filtered, washed with methanol and diethyl ether, dried under vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2005.03.051