acide cis-N-tosyl perhydrocyclopentapyrrole-2-carboxylique

Base Information

• Chemical Name: acide cis-N-tosyl perhydrocyclopentapyrrole-2-carboxylique
• CAS No.: 134786-35-9
• Molecular Formula: C₁₅H₁₉NO₄S
• Molecular Weight: 309.386

Synonyms:

Chemical Property of acide cis-N-tosyl perhydrocyclopentapyrrole-2-carboxylique

Chemical Property:

Purity/Quality:

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Technology Process of acide cis-N-tosyl perhydrocyclopentapyrrole-2-carboxylique

There total 20 articles about acide cis-N-tosyl perhydrocyclopentapyrrole-2-carboxylique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

cis-N-tosyl perhydrocyclopentapyrrole-2-methanol (134786-22-4,134877-18-2,134877-19-3) → acide cis-N-tosyl perhydrocyclopentapyrrole-2-carboxylique (134786-35-9,134877-21-7,134877-22-8)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; water; In acetone; a) -5 deg C, 3 h, b) room temperature, 5 h;

DOI:10.1016/S0040-4020(01)96036-3

Reference yield: 89.0%

cis-N-tosyl perhydrocyclopentapyrrole-2-methanol (134786-22-4,134877-18-2,134877-19-3) → acide cis-N-tosyl perhydrocyclopentapyrrole-2-carboxylique (134786-35-9,134877-21-7,134877-22-8)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; water; In acetone; a) -5 deg C, 3 h, b) room temperature, 5 h;

DOI:10.1016/S0040-4020(01)96036-3

Reference yield: 77.0%

(2RS,3aSR,6aRS)-N-tosyl perhydrocyclopentapyrrole-2-methanol (134786-22-4,134877-18-2,134877-19-3) → acide (2RS,3aSR,6aRS)-N-tosyl perhydrocyclopentapyrrole-2-carboxylique (134786-35-9,134877-21-7,134877-22-8)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; water; In acetone; a) -5 deg C, 3 h, b) room temperature, 5 h;

DOI:10.1016/S0040-4020(01)96036-3

upstream raw materials:

cis-N-tosyl perhydrocyclopentapyrrole-2-methanol

2-(2-propenyl)cyclopentylamine

(E)-2-allylcyclopentanone oxime

cis-1-N-tosyl-2-(2-propenyl)cyclopentylamine

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