Technology Process of 13-decyl-13-heptyltritriacontane
There total 5 articles about 13-decyl-13-heptyltritriacontane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydrogensulfate;
at 160 ℃;
unter vermindertem Druck und Hydrieren des erhaltenen Olefin-Gemisches an Raney-Nickel in Methylcyclohexan bei 180grad/220 at;
DOI:10.1021/jo01094a035
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diethyl ether / und beim Behandeln der Reaktionsloesung mit wss.Salzsaeure
2: lithium alanate; diethyl ether
3: potassium hydrogen sulfate / 160 °C / unter vermindertem Druck und Hydrieren des erhaltenen Olefin-Gemisches an Raney-Nickel in Methylcyclohexan bei 180grad/220 at
With
potassium hydrogensulfate; lithium aluminium tetrahydride; diethyl ether;
DOI:10.1021/jo01094a035
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium alanate; diethyl ether
2: potassium hydrogen sulfate / 160 °C / unter vermindertem Druck und Hydrieren des erhaltenen Olefin-Gemisches an Raney-Nickel in Methylcyclohexan bei 180grad/220 at
With
potassium hydrogensulfate; lithium aluminium tetrahydride; diethyl ether;
DOI:10.1021/jo01094a035