Ag(OClO₃)(P(C₆H₅)3)2

Base Information

Chemical Name:Ag(OClO₃)(P(C₆H₅)3)2
CAS No.:86730-74-7
Molecular Formula:C₃₆H₃₀AgClO₄P₂
Molecular Weight:731.901
Hs Code.:

Ag(OClO<sub>3</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)2

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ag(OClO₃)(P(C₆H₅)3)2

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Technology Process of Ag(OClO₃)(P(C₆H₅)3)2

There total 10 articles about Ag(OClO₃)(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: silver perchlorate

: 86730-74-7,154965-03-4
Ag(OClO₃)(P(C₆H₅)3)2

Guidance literature:: With triphenylphosphine; In acetone; PPh3 was added to a soln. of AgClO4 in acetone, mixt. was stirred for 30 min in the absence of light; solvent was removed in vacuo, residue dissolved in CH2Cl2, ether added, resulting crystals were filtered off, washed with ether, dried in vacuo; elem. anal.;
DOI:10.1016/S0022-328X(00)98835-1

Reference yield: 40.0%

: C₆Cl₅Ni(P(C₆H₅)3)2Cl

: silver perchlorate

: 86730-74-7,154965-03-4
Ag(triphenylphosphine)₂ perchlorate

: 78331-77-8
[Ni(pentachlorophenyl)(pyridine)3]ClO₄

Guidance literature:: With pyridine; In benzene; byproducts: AgCl; addn. of stoich. amt. of AgClO4 to Ni-complex, filtration off of Ag-compds., addn. of pyridine;
DOI:10.1016/S0020-1693(00)90072-0

Reference yield:

: (C₈H₁₂)Rh(C₇H₄N₂C₅H₄N)Ag(P(C₆H₅)3)⁽¹⁺⁾*ClO₄^(1-)=((C₈H₁₂)Rh(C₇H₄N₂C₅H₄N)Ag(P(C₆H₅)3))ClO₄

: 86730-74-7,154965-03-4
Ag(OClO₃)(P(C₆H₅)3)2

: ((CO)2Rh(C₇H₄N₂C₅H₄N))2Ag⁽¹⁺⁾*ClO₄^(1-)=(((CO)2Rh(C₇H₄N₂C₅H₄N))2Ag)ClO₄

Guidance literature:: With carbon monoxide; In dichloromethane; byproducts: cycloocta-1,5-diene; dry CO was bubbled through a soln. of Rh-complex in CH2Cl2 for 1 h, the mixt. was kept for 2 h at -10°C; ppt. (Rh-complex) was filtered off, washed with cold CH2Cl2, dried in vacuo, filtrate was concd. in vacuo, ether added, resulting ppt. was twice recrystd. from CH2Cl2-ether and showed (IR spect.) to be a mixt. of Ag(OClO4)(PPh3)2 and unidentified deriv.;
DOI:10.1016/S0022-328X(00)98835-1